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EPD 방법을 이용한 알루미나-실리카 복합 코팅막의 제조와 전기절연 특성

Preparation of Alumina-Silica Composite Coatings by Electrophoretic Deposition and their Electric Insulation Properties

  • 지혜 (한국세라믹기술원 에너지환경소재본부) ;
  • 김두환 (한국세라믹기술원 에너지환경소재본부) ;
  • 박희정 (한국세라믹기술원 에너지환경소재본부) ;
  • 임형미 (한국세라믹기술원 에너지환경소재본부) ;
  • 이승호 (한국세라믹기술원 에너지환경소재본부) ;
  • 김대성 (한국세라믹기술원 에너지환경소재본부) ;
  • 김영희 (한국세라믹기술원 에너지환경소재본부)
  • Ji, Hye (Energy & Environmental Division, Korea Institute of Ceramic Engineering & Technology) ;
  • Kim, Doo Hwan (Energy & Environmental Division, Korea Institute of Ceramic Engineering & Technology) ;
  • Park, Hee Jeong (Energy & Environmental Division, Korea Institute of Ceramic Engineering & Technology) ;
  • Lim, Hyung Mi (Energy & Environmental Division, Korea Institute of Ceramic Engineering & Technology) ;
  • Lee, Seung-Ho (Energy & Environmental Division, Korea Institute of Ceramic Engineering & Technology) ;
  • Kim, Dae Sung (Energy & Environmental Division, Korea Institute of Ceramic Engineering & Technology) ;
  • Kim, Younghee (Energy & Environmental Division, Korea Institute of Ceramic Engineering & Technology)
  • 투고 : 2013.09.30
  • 심사 : 2014.03.07
  • 발행 : 2014.05.31

초록

Alumina-silica composite coating layers were prepared by electrophoretic deposition (EPD) of plate-shaped alumina particles dispersed in a sol-gel binder, which was prepared by hydrolysis and the condensation reaction of methyltrimethoxysilane in the presence of colloidal silica. The microstructure and the electrical and thermal properties of the coatings were compared according to the EPD process parameter: voltage, time and the content of the plate-shaped alumina particles. The electrical insulation property of the coatings was measured by a voltage test. The coatings were prepared by EPD of the sol-gel binder with 5-30 wt% plate alumina particles on parallel electrodes at a distance of 2 cm for 1-10 min under an applied voltage of 10-30 V. The coatings experienced increased breakdown voltage with increasing thickness. However, the higher the thickness was, the smaller the breakdown voltage strength was. A breakdown voltage as high as 4.6 kV was observed with a $400{\mu}m$ thickness, and a breakdown voltage strength as high as 27 kV/mm was achieved for the sample under a $100{\mu}m$ thickness.

키워드

참고문헌

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피인용 문헌

  1. Preparation and Characterization of Organic-inorganic Hybrid Composite Film with Plate-shaped Alumina by Electrophoretic Deposition as a Function of Aging Time of Sol-Gel Binder vol.52, pp.5, 2015, https://doi.org/10.4191/kcers.2015.52.5.366
  2. 표면전하 거동 조절을 이용한 탈크-실리카 복합체의 제조 vol.34, pp.1, 2014, https://doi.org/10.12925/jkocs.2017.34.1.116
  3. 층간 삽입반응으로 얻어진 화합물을 이용한 휘발성 유기화합물의 흡착과정 변화에 대한 연구 vol.34, pp.4, 2014, https://doi.org/10.12925/jkocs.2017.34.4.799