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Hardness Analysis of Surface Treated Magnesium Alloy using Laser Induced Breakdown Spectroscopy

레이저 플라즈마 분광분석법을 이용한 표면처리 된 마그네슘 합금 표면의 경도 분석

  • Kang, Dongchan (Department of Mechanical Engineering, The Graduate School, Seoul Nat'l Univ. of Science & Technology) ;
  • Kim, Joohan (Department of Mechanical & Automotive Engineering, Seoul Nat'l Univ. of Science & Technology)
  • Received : 2015.08.15
  • Accepted : 2015.12.08
  • Published : 2015.12.15

Abstract

The hardness of surface treated magnesium alloy was evaluated using laser induced breakdown spectroscopy. The surface of the specimen was hardened mechanically, and the hardness profiles were measured using a traditional measurement technique. A laser beam was irradiated to generate a plasma, and the peaks of the components of the specimen were analyzed. A wavelength of 333.66 nm and 293.65 nm were selected as the atomic and ionic peaks, respectively. The ratios of the ionic peak to the atomic peak were obtained so as to compare the hardness profile. As the depth increased, the ratio decreased. These results are in good agreement with the previous hardness measurement results. It can be considered that this technique could be applied for remote and time-efficient hardness measurement.

Keywords

References

  1. Aguilera, J. A., Aragon, C., Maduraga, V., Manrique, J., 2009, Study of Matrix Effects in Laser Induced Breakdown Spectroscopy on Metallic Samples Using Plasma Characterization by Emission Spectroscopy, Spectrochimica Acta Part B, 64:10 993-998. https://doi.org/10.1016/j.sab.2009.07.007
  2. Senesi, G. S., 2014, Laser Induced Breakdown Sepctroscopy (LIBS) Applied to Terrestrial and Extraterrestrial Analogue Geomaterials with Emphasis to Minerals and Rocks, Earth-science Reviews, 139 231-267.
  3. Gomes, M. D. S., Carvalho G. G. A. D., Junior, D. S., Krug F. J., 2013, A Novel Strategy for Preparing Calibration Standards for The Analysis of Plant Materials by Laser-induced Breakdown Spectroscopy: A Case Study with Pellets of Sugar Cane Leaves, Spectrochimica Acta Part B, 86 137-141. https://doi.org/10.1016/j.sab.2013.03.009
  4. Melessanaki, K., Mateo, M., Ferrence, S. C., Betancourt P. P., Anglos, D., 2002, The Application of LIBS for The Analysis of Archaeological Ceramic and Metal Artifacts, Applied Surface Science, 197-198 156-163. https://doi.org/10.1016/S0169-4332(02)00459-2
  5. Sun, L., Yu, H., 2009, Correction of Self-absorption Effect in Calibration-Free Laser-Induced Breakdown Spectroscopy by an Internal Reference Method, Talanta, 79:2 388-395. https://doi.org/10.1016/j.talanta.2009.03.066
  6. Ferreira, E. C., Milori, D. M. B. P., Ferreira, E. J., Santos, L. M. D., Martin-Neto, L., Nogueira, A. R. D. A., 2011, Evaluation of Laser Induced Breakdown Spectroscopy for Multielemental Determination in Soils Under Sewage Sludge Application, Talanta, 85:1 435-440. https://doi.org/10.1016/j.talanta.2011.04.001
  7. Li, J., Lu, J., Dai, Y., Dong, M., Zhong, W., Yao, S., 2015, Correlation between Aging Grade of T91 Steel and Spectral Characteristics of The Laser-induced Plasma, Applied Surface Science, 346 302-310. https://doi.org/10.1016/j.apsusc.2015.03.186
  8. Ko, C., Lee, W., Kim, J., 2013, Measurement of Stress of Ti6Al4V by Laser Induced Breakdown Spectroscopy, Conf. Proc. of The Korean Society of Manufacturing Technology Engineers, 10 253-253.
  9. Wang, Z., Li, L., West, L., Li, Z., Ni, W., 2012, A Spectrum Standardization Approach for Laser-induced Breakdown Spectroscopy Measurements, Spectrochimica Acta Part B, 68 58-64. https://doi.org/10.1016/j.sab.2012.01.005
  10. Mohamed, W. T. Y., 2007, Study of The Matrix Effect on The Plasma Characterization of Six Elements in Aluminum Alloys Using LIBS with A Portable Echelle Spectrometer, Progress In Physics, 2 42-49.
  11. Messaoud Aberkane, S., Bendib, A., Yahiaoui, K., Boudjemai, S., Abdelli-Messaci, S., Kerdja, T., Amara, S. E., Harith, M. A., 2014, Correlation between Fe-V-C Alloys Surface Hardness and Plasma Temperature via LIBS Technique, Applied Surface Science, 301 225-229. https://doi.org/10.1016/j.apsusc.2014.02.046
  12. Cowpe, J. S., Moorehead, R. D., Astin, J. S., Karthikeyan, S., Kilcoyne, S. H., Crofts, G., Pilkington, R. D., 2011, Hardness Determination of Bio-ceramics Using Laser-induced Breakdown Spectroscopy, Spectrochimica Acta Part B: Atomic Spectroscopy, 66:3-4 290-294. https://doi.org/10.1016/j.sab.2011.03.007
  13. Shahdad, S. A., Mccabe, J. F., Bull, S., Rusby, S., Wassel, R. W., 2007, Hardness Measured with Traditional Vickers and Martens Hardness Methods, Dental Materials, 23:9 1079-1085. https://doi.org/10.1016/j.dental.2006.10.001
  14. Kim, J., Ko, C., 2013, Non-contact Measurement and Analysis of Surface Hardness on Welding Steel Using Laser-induced Breakdown Spectroscopy, Journal of The Korean Society for Precision Engineering, 31:2 141-148. https://doi.org/10.7736/KSPE.2014.31.2.141
  15. Abdel-Salam, Z. A., Galmed, A. H., Tognoni, E., Harith, M. A., 2007, Estimation of Calcified Tissues Hardness via Calcium and Magnesium Ionic to Atomic Line Intensity Ratio in Laser Induced Breakdown Spectra, Spectrochimica Acta Part B: Atomic Spectroscopy, 62:12 1343-1347. https://doi.org/10.1016/j.sab.2007.10.033
  16. Pyoun, Y. S., Cho, I. S., Lee, C. S., Park, I. G., Kim, D. S., Kim, C. S., Cho, I. H., 2007, Application of Ultrasonic Nano-Crystal Surface Modification Technology Which Realizes Simultaneous Improvement of Fatigue Strength with Peening Effect and Improvement of Wear Resistance and Friction Loss with Case Hardening and Micro Dimples Surface Topology, The Korean Society of Manufacturing Technology Engineers, 5 346-354.
  17. Yu, J. I., Yoon, J. S., Yun, J. G., Kim, J. J., Choi, S. D., 2012, The Study of Part Surface Treatment in Magnesium Alloy, The Korean Society of Manufacturing Technology Engineers, 4 194-194.

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