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Setting Time Evaluation of Concrete Using Electrical Resistivity Measurement

전기비저항 측정을 이용한 콘크리트 응결시점 평가

  • Lee, Han Ju (Dept. of Construction and Disaster Prevention Engineering, Kyungpook National University) ;
  • Yim, Hong Jae (Dept. of Construction and Disaster Prevention Engineering, Kyungpook National University)
  • 이한주 (경북대학교 건설방재공학부) ;
  • 임홍재 (경북대학교 건설방재공학부)
  • Received : 2017.01.22
  • Accepted : 2017.06.14
  • Published : 2017.08.31

Abstract

Setting time of cement-based materials can represent a developing strength in early-age mixture, and it can be used a significant parameter of high-performance concrete having various mix-proportions. Generally, initial and final setting time of concrete is measured by penetration resistance method that used a wet-sieving mortar mixture, therefore, it hardly represents the setting time of sound concrete including coarse aggregate. Recently, several nondestructive methods, such as ultrasonic velocity and impendence measurement, are proposed to evaluate the setting time of fresh concrete. This study attempts to measure an electrical resistivity using four-electrode method for evaluation of setting time in early-age cement-based materials. For this purpose, total 10 mixtures are prepared as different mix-proportions including chemical admixture. Based on the experimental results, two electrical parameters, such as initial electrical resistivity and rising time, are proposed to reflect a microstructure development by hydration of cement-based materials. As a result, proposed parameter is also discussed with the measured setting time by penetration resistance method.

고성능 콘크리트의 개발로 인해 다양해지는 배합비에 따라, 콘크리트 초기강도 발현 시점을 예측할 수 있는 응결시점에 대한 관심이 높아지고 있다. 기존의 콘크리트 응결시간 측정을 위해 사용되고 있는 관입저항시험은 습식체가름을 실시한 모르타르를 이용한 간접적인 측정법으로, 현장 타설된 콘크리트의 정확한 응결시간을 나타내기 어렵다. 따라서 콘크리트에 직접 측정이 가능한 초음파 속도 측정법, 수화열 측정법, 전기 임피던스 측정법 등 다양한 비파괴 평가 기법들이 제안되고 있다. 본 연구에서는 수화 반응에 따른 시멘트계 재료 내부 전기전도성 변화를 측정하는 4-전극법을 이용하여 콘크리트의 전기 비저항 측정 기법을 제안하고자 한다. 다양한 배합비에 따라 시멘트 페이스트, 모르타르, 콘크리트의 전기 비저항 측정을 실시하였으며, 배합 후 24시간 측정결과로부터 초기 전기비저항 값과 전기비저항 상승시기를 측정 변수로 제안하였다. 또한, 관입 저항 시험에 따른 초결, 종결 시점과의 비교 분석을 통해 콘크리트 응결시점 평가를 위한 제안 기법의 적용 가능성을 확인하였다.

Keywords

Acknowledgement

Supported by : 한국연구재단

References

  1. Kwon, S. J., Song, H. W., Byun, K. J., and Lee, S. H., "Analysis of Carbonation Behavior of Creacked Concrete in Early-age", Journal of the Korean Society of Civil Engineers, Vol. 24, No. 5A, 2004, pp. 1011-1022.
  2. Lee, S. B., Yang, J. M., Choi, S. H., Kim, S. H., and Shin, K. J., "Measurements of Setting Time for Fiber Reinforced Mortar", Proceedings of Korean Society of Civil Engineers Conference, Korean Society of Civil Engineers, Daegu, Korea, 2014, pp. 1205-1206.
  3. Lee, S. H., Lim, Y. J., and Cho. J. W., "Hydration Properties of Ordinary Portland Cement Using Mixture of Limestone and Blast Furnace Slag as Minor Inorganic Additives", Journal of the Korea Concrete Institute, Vol. 27, No. 1, 2015, pp. 3-9. https://doi.org/10.4334/JKCI.2015.27.1.003
  4. Neville, A. M., Properties of Concrete, Longman, London, 1995.
  5. Mindess, S., Young, J. F., and Darwin, D., Concrete, Prentice Hall, New Jersey, 2003, pp. 210-213.
  6. Han, M. C., "Effect of the Curing Temperature on Autogenous Shrinkage of the High Strength Mortar incorporating Mineral Admixture", Journal of the Korean Recycled Construction Resources Institute, Vol. 6, No. 4, 2011, pp. 127-133.
  7. Lee, S. S., Song, H. Y., and Lee, S. M, "An Experimental Study on the Influence of High Fineness Fly Ash and Water-Binder Ration on Properties of Concrete", Journal of the Korea Concrete Institute, Vol. 21, No. 1, 2009, pp. 29-35. https://doi.org/10.4334/JKCI.2009.21.1.029
  8. KS I 5108, Testing Method for Setting time of Hydraulic Cement by Vicat Needle, Korean Agency for Technology and Standards, Seoul, Korea, 2007, pp. 1-11.
  9. ASTM Standards, ASTM C403/C403M Standard Test Method for Time of Setting of Concrete Mixtures by Penetration Resistance, ASTM, USA, pp. 1-7.
  10. Chung, C. W., Suraneni, P., Popovice, J. S., and Struble, L. J., "Setting Time Measurement Using Ultrasonic Wave Flection", ACI Materials of Concrete Journal, Vol. 109, No. 1, 2012, pp. 109-118.
  11. Trtnik, Gregor, Marko I. Valic, and Goran Turk., "Measurement of Setting Process of Cement Pastes Using Non-destructive Ultrasonic Shear Wave Reflection Technique", NDT & E International, Vol. 56, 2013, pp. 65-75. https://doi.org/10.1016/j.ndteint.2013.02.004
  12. Yim, H. J., Kim, J. H., and Shah, S. P., "Ultrasonic Monitoring of the Setting of Cement-Based Materials: Frequency Dependence", Construction and Building Materials, Vol. 65, 2014, pp. 518-525. https://doi.org/10.1016/j.conbuildmat.2014.04.128
  13. Pinto, R. C. A. and Hover, K. C., "Application of Maturity Approach to Setting Times", Materials Journal, Vol. 96, No. 6, 1999, pp. 686-691.
  14. Canno, N. J., "Nondestructive Testing of Concrete: History and challenges", SP 144- 30. In: Mehta PK, editor. Concrete technology - past, present and future. ACI, Detroit, MI, 1994, pp. 624-678.
  15. Valic, M. I., "Hydration of Cementitious Materials by PulseEcho USWR: Method, Apparatus and Application Examples", Cement and Concrete Research, Vol. 30, No. 10, 2000, pp. 1633-1640. https://doi.org/10.1016/S0008-8846(00)00352-5
  16. Hamann, C. H., Hamnett, A., and Vielstich, W., "Electrochemistry", Wiley-VCH, USA, 1998, pp. 2-31.
  17. Hwang, G. R. and Shin, S. W., "Setting Monitoring of Hydration Cement-based Materials Using Electrical Impedance Spectroscopy", Proceedings of Korean Society of Civil Engineers Conference, Korean Society of Civil Engineers, Gwangju, Korea, 2012, pp. 2449-2452.
  18. Shin, S. W., Hwang, G. R., and Lee, C. J., "Electrical Impedance Response Model of Concrete in Setting Process", Journal of the Korean Society of Safety, Vol. 29, No. 5, 2014, pp. 116-122. https://doi.org/10.14346/JKOSOS.2014.29.5.116
  19. Lee, B. H. and Lee, S. C., "Major Foundational Technics for Grounding Systems", Uije Publication Ltd, Seoul, 1999, pp. 45-51.
  20. Campo, M. A., Woo, L. Y., Mason, T. O., and Garboczi, E. J., "Frequency-Dependent Electrical Mixing Law Behavior in Spherical Particle Composites" Journal of Electroceramics, Vol. 9, No. 1, 2002, pp. 49-56. https://doi.org/10.1023/A:1021642118889
  21. Wang, Z., Zeng, Q., Wang, L., Yao, Y., and Li, K., "Electrical Resistivity of Cement Pastes Undergoing Cyclic Freeze-thaw Action", Journal of Materials in Civil Engineering, Vol. 27, No. 1, 2014, 04014109. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001042
  22. Spragg, R., Jones, S. Z., Villani, C., Snyder, K. A., Bentz, D. P., Poursaee, A., and Weiss, J., "Surface and Uniaxial Electrical Measurements on Layered Cementitious Composites having Cylindrical and Prismatic Geometries", International Conference on the Durability of Concrete Structure, Indiana, 2014, pp. 317-326.
  23. Topcu, I. B., Uygunoglu, T., and Hocaoglu, I., "Electrical Conductivity of Setting Cement Paste with Different Mineral Admixtures", Construction and Building Materials, Vol. 28, No. 1, 2012, pp. 414-420. https://doi.org/10.1016/j.conbuildmat.2011.08.068
  24. Wenner, F., "A Method of Measuring Earth Resistivity", Journal of the Franklin Institute, Vol. 180, No. 3, 1915, pp. 373-375. https://doi.org/10.1016/S0016-0032(15)90298-3
  25. KS I ISO 679, Methods of Testing Cement-Determination of Strength, Korean Agency for Technology and Standard, Seoul, Korea, 2006, pp. 1-16.