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Effect of Multi-Sized Powder Mixture on Solid Casting and Sintering of Alumina

  • Cho, Kyeong-Sik (School of Advanced Materials Science and Engineering, Kumoh National Institute of Technology) ;
  • Lee, Hyun-Kwuon (School of Advanced Materials Science and Engineering, Kumoh National Institute of Technology) ;
  • Min, Jae-Hong (School of Advanced Materials Science and Engineering, Kumoh National Institute of Technology)
  • 투고 : 2018.03.25
  • 심사 : 2018.04.26
  • 발행 : 2018.07.31

초록

The slip casting process is widely used to make green bodies from ceramic slips into dense compacts with homogeneous microstructure. However, stress may be generated inside the green body during drying, and can lead to cracking and bending during sintering. When starting from the spherical powders with mono-size distribution to make the close packed body, interstitial voids on octahedral and tetrahedral sites are formed. In this research, experiments were carried out with powders of three size types (host powder (H), octahedral void filling powder (O) and tetrahedral void filling powder (T)) controlled for average particle size by milling from two commercial alumina powders. Slips were prepared using three different powder batches from H only, H+O or H+O+T mixed powders. After manufacturing green compacts by solid-casting, compacts were dried at constant temperature and humidity and sintered at $1650^{\circ}C$. Alumina samples fabricated from the multi-sized powder mixture had improved compacted and sintered densities.

키워드

참고문헌

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피인용 문헌

  1. Reducing the density deviation in alumina by pressure-vacuum hybrid slip casting by employing powders with different particle sizes vol.8, pp.2, 2018, https://doi.org/10.1080/21870764.2020.1749372
  2. Modification of a low-soda easy-sintered α-Al2O3 powder for the application in semiconductor/display production equipment vol.38, pp.12, 2018, https://doi.org/10.1007/s11814-021-0915-0