• Title/Summary/Keyword: Exhaust dyeing

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The Studies of Low Temperature Dyeing on Silk Fibers I. Low Temperature Dyeing of Silk Fiber in the Milling Type Acid Dye (견의 저온 염색에 관한 연구 I. 산성 Milling형 염색에 있어서의 저온염색)

  • 배도규;배현석;정태암
    • Journal of Sericultural and Entomological Science
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    • v.34 no.2
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    • pp.52-57
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    • 1992
  • Using the new type auxiliary(K-1), dyeing experiment was done at the various dyeing conditions and the effects of auxiliary on the dyeing properties of acid milling dye for the silk fiber were dicussed. The results obtained were as follows; 1. The exhaust rate of acid milling dye was increased according to the auxiliary concentration at dyebath pH 7, But the increasing tendency of exhaust rate was decreased above auxiliary concentration 3% o. w. f.. 2. It was the same tendency of exhaust rate at dyebath pH 5, but the diffusion was more powerful at dyebath pH 7 than pH 5. 3. The decreasing ratio of exhaust rate according to dye concentration increasing was lower at auxiliary addition than auxiliary non-addition. 4. The exhaust rate curve according to increasing dyeing temperature showed the inflection point at auxiliary non-addition, but it was not observed in auxiliary addition. Consequently, it seems to be avoid that the occurrence of uneven dyeing at auxiliary addition.

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Studies of Low Temperature Dyeing on Silk Fiber II. Low Temperature Dyeing of Silk Fiber with the Complex Dye (견의 저온염색에 관한 연구 II. 산성 Metal Complex 염료에 있어서의 저온염색)

  • 배도규;배현석
    • Journal of Sericultural and Entomological Science
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    • v.35 no.1
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    • pp.48-51
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    • 1993
  • Using the new type auxiliary(K-1), dyeing experiment was done at the various dyeing conditions and the effects of auxiliary on the dyeing properties of metal complex dye for the silk fiber were dicussed. The exhaust rate was higher in the auxiliary 3% o.w.f. addition than sodium sulfate 50% o.w.f. The decreasing ratio of exhaust rate according to dye concentration increasing was lower at auxiliary addition than auxiliary non-addition. The exhaust rate according to increasing dyeing temperature was higher in the auxiliary addition than non-addition.

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A Study on the One Bath Two Step Dyeing of Nylon/ Cationized Cotton Blends with Acid Dye/Direct Dye (나일론/카티온화 면 혼방품의 산성염료/직접염료에 의한 1욕 2단 염색에 관한 연구)

  • 성우경
    • Textile Coloration and Finishing
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    • v.12 no.1
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    • pp.44-51
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    • 2000
  • The conventional one bath exhaust dyeing system of nylon]/cotton blends with acid dye/direct dye involves a lot of neutral salt which affect dyeability of acid dyes. Because of conventional one bath exhaust dyeing system of nylonl/cotton blends with acid dye/direct dye needs acid dyes adjusted at a neutral liquor, suitable acid dye is limited. To improve dyeing property of nylon/cotton blends, cotton component was pretreated with cationizing agent containing chlorohydrine group in aqueous solution of sodium hydroxide. This study was carried out to investigate dyeing possibilities of nylon/cationized cotton blends with acid dye/direct dye in a non-neutral salt dyebath by one bath two step method. The concentration of direct dye was 1.0%, 0.7%, 0.3%o.w.f. respectively at a non, 1%, 3%owf of reserving agent for being almost equal color strength between nylon and 3% cationized cotton when nylon/3% cationized cotton blends was dyed with acid dye/direct dye at concentration of acid dye(1%o.w.f.) by one bath two step method.

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Studies on the One Bath Exhaust Dyeing System of Polyester/Cationized Cotton Blends with Disperse Dye/Reactive Dye (폴리에스테르/카티온화 면 혼방품의 분산염료/반응성염료에 의한 일욕염색계에 관한 연구)

  • 성우경
    • Textile Coloration and Finishing
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    • v.10 no.2
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    • pp.18-28
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    • 1998
  • in order to overcome disadvantage of the conventional two bath dyeing method of polyester/cotton blends, it had prompted significant effort to the development of the one bath dyeing method which can accomplish sayings in time, energy and water usage. Also, when dyeing polyester/cotton blends by the one bath dyeing method, the high salt concentrations needed for the reactive dye can cause particles of disperse dye, used for the polyester component, to aggregate. A supplementary problem that can occasionally be happened is the change of hue that occurs on dyed polyester in an alkaline dyebath. To improve dyeing property of polyester/cotton blends, cotton component was pretreated with epichlolohydrine-trimethylamine hydrochloride in aqueous solution of sodium hydroxide to produce a cationized cotton that can be dyed under neutral conditions with reactive dye in a non-electrolytic or il little electrolytic dyebath. The one bath dyeing method of polyester/cationized cotton blends with disperse dye/reactive dye mixture resulted in a satisfactory dyeing property and color yield in comparison with ordinary two bath dyeing method.

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Preparation of Nano Disperse Dyes from Nanoemulsions and Their Dyeing Properties on Ultramicrofiber Polyester

  • Choi Jae-Hong;Kang Min-Ju
    • Fibers and Polymers
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    • v.7 no.2
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    • pp.169-173
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    • 2006
  • Six nano disperse dyes were prepared using corresponding O/W nanoemulsions which were obtained with sodium laurylsulphate and caprylic triglyceride. The average particle size of the dyes prepared were in the range of $110{\sim}130nm$. Exhaust dyeing using nano dyes resulted in low exhaustion yields of $17{\sim}26%$ on regular polyester fiber and $28{\sim}38%$ on ultramicrofiber polyester. The observed low exhaustion yields of nano disperse dye can be explained by the solubilization of dye particles into surfactant micelles as well as the high stability of the nanoemulsions, these might reduce the capacity of dye uptake onto the fibers. However, higher K/S values of dyeings with nano dyes on ultramicrofiber sites compared to those on regular polyester sites suggested their potential to be more efficient dyes for finer denier microfiber polyesters.

A Study of Dyeability at Low Temperature on the Ultra-microfiber (해도사의 저온염색성에 대한 고찰)

  • 장지은;강민주;최재홍
    • Textile Coloration and Finishing
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    • v.16 no.3
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    • pp.8-13
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    • 2004
  • This research aimed at scrutinizing the comparative dyeability of some disperse dyes at low temperature on ultra-microfiber polyester, islands in the sea type (0.05 denier), which has claimed utmost fastness and improved uptake of dyeing. Comparisons of dyeability, such as rate of dyeing and color depth, on ultra-microfiber polyester were evaluated by H.T. exhaust dyeing method and followed by the test of rubbing fastness. To achieve high wet fastness, some commercial disperse dyes, Terasil WW and Megacron dyes, which have been recently launched for excellent wash fastness, have been examined compared with conventional disperse dyes, C.I Disperse Red 167 and C.I Disperse Orange 30.

Dyeing of high Light Fastness Solvent Dyes on Polyester Fiber (고 일광견뢰도 Solvent 염료의 폴리에스터 염색에 관한 연구)

  • 최재홍
    • Textile Coloration and Finishing
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    • v.15 no.3
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    • pp.176-184
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    • 2003
  • This research aimed at scrutinizing the dyeability of some solvent dyes on polyester and their light fastness to be exploited as a breakthrough in light fastness where utmost fastness is required such as ultramicrofibers and industrial markets. Dyeability on polyester was mainly evaluated by HT exhaust dyeing according to the general procedure. Light fastness has been tested by a preliminary UV test followed by HT xenon test in compliance with standard SAE J1885, 224 KJ. Fading has been determined quantitatively by evaluating the shade deviation and the strength difference between unexposed and exposed samples by means of CIELab values.

Dyeability of Low-melting Hybrid Polyester at Low Temperature (저융점 폴리에스테르 복합사의 저온 염색성)

  • Hwang, Ji-Hyun;Kim, Chang-Nam;Ma, Jin-Suk;Oh, Hae-Sun;Yoon, Nam-Sik
    • Textile Coloration and Finishing
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    • v.24 no.2
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    • pp.113-120
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    • 2012
  • Jacquard floor covering could be prepared from low-melting/regular sheath-core hybrid polyester, where the fiber is dyed in yarn state. With regard that the expected high shrinkage of the hybrid polyester in water makes problems in yarn dyeing, low-temperature dyeing properties of the hybrid polyester were studied. The rate of shrinkage of low-melting hybrid polyester exceeds 9% in hot water above $90^{\circ}C$, at such condition, cheese yarn dyeing is very difficult. Although disperse dyes exhaust in a relatively high speed on low-melting hybrid polyester, diffusion of these dyes to the core regular polyester was extremely slow under $90^{\circ}C$. Foron Blue E-BL 150, an anthraquinone E-type disperse dye, showed appreciable diffusion after 48hrs dyeing at $90^{\circ}C$. The fastness to rubbing and drycleaning were improved by one grade after reduction cleaning.

Synthesis of novel disperse dyes derived from phthalimide containning diester groups and their dyeing properties

  • Choi, Jae-Hong;Choi, Jong-Yun;Lee, Hyun-Young;Kwon, Oh-Tak
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2009.03a
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    • pp.45-46
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    • 2009
  • In this study, 12 azo disperse dyes based on phthalimide were synthesized including their precursors. The chemical structures of the dyes and the corresponding precursors were analyzed by the GC-MASS, $^1H$ NMR spectra and elemental analysis. The dyeability on PET, such as step dyeing and build-up properties and color fastness were examined using conventional exhaust dyeing procedures.

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Dyeing Properties of Polyurethane Fiber by Novel Phthalimidyl Azo Disperse Dyes (Phthalimide계 신규 Azo dye의 Polyurethane계 섬유 염색 특성)

  • Choi, Jong-Yun;Choi, Jae-Hong
    • Textile Coloration and Finishing
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    • v.21 no.6
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    • pp.46-55
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    • 2009
  • Some phthalimidyl azo dyes containing N,N-diethyl or N,N-di($\beta$-methoxycarbonylethyl) group have been attempted to apply onto two kinds of polyurethane based materials and rationalize their dyeability and fastness comparing with those of some commercial disperse dyes. Phthalimidyl azo dye showed 66~98% of exhaustion yield at $120^{\circ}C$ by a conventional exhaust dyeing method. The dyeings were found to have a higher wash fastness with both fabrics in comparison with those of commercial dyes which indicates lower thermomigration and efficient alkali clearable properties of phthalimidyl ring and/or diester group during post-dyeing process.