• 동력기계공학회지
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• 제16권1호
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• pp.72-77
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• 2012

Acoustic emission (AE) is known to be sensitive to fracture process and so it was expected that AE data may propose as a means of monitoring the fracture information. The aim of this study is to analyze the characteristic of AE signal emitted from glass during Vickers indentation. To observe AE characteristics by surface effect, both glass and coating glass were studied. During Vickers indentation loading, AE signal resulted from penny-like crack is detected. During Vickers indentation unloading, AE signal resulted from both radial/median crack and lateral crack is detected. In case of indentation on glass, the emission energy(${\epsilon}$) is found to be approximately proportional to the fourth power of the crack length. In case of indentation on coating glass, the emission energy(${\epsilon}$) is approximately proportional to the crack length.

• The Korean Journal of Ceramics
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• 제5권2호
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• pp.119-124
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• 1999

Silicon nitride ceramics with highly oriented microstructure were prepared by tape casting a slurry containing 5 wt% of the silicon nitride whiskers. The whiskers were aligned in the casting direction and worked as seeds for the grain growth. The anisotropy was observed from the sintering shrinkage, Vickers indentation crack lengths, and XRD patterns. The cracks were much longer on the surface normal to the aligned grains than on the tape casting surface where the lateral cracks were also observed. The effect of sintering additives and the annealing treatment on the indentation crack length was examined. The sample with higher silica content had longer cracks than the one with lower silica content. The crack length anisotropy increased after annealing at 2123K.

• 한국정밀공학회지
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• 제12권2호
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• pp.5-13
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• 1995

Various techniques to measure fracture toughness which is an important parameter to predict fracture behavious of structural materials have been reported. Among these mathods, this paper describes the micro-Vickers indentation crack method to estimate the fracture toughness of some WC-Co composites. Two indentation crack patterns (such as radial-median cracks (orhalf-penny cracks) and Palmqvist cracks generated during indentation) are referred precisely. The fracture toughness of WC-4.7wt%Co, WC-6wr%Co and WE-9wr%Co composites were estimated by using some equations given by Shetty et al., Nihara et al. in this study. We show the reliability of indentation method by comparing the results with those from literatures. The appropriate equation to estimate the fracture toughness in the case of WC-Co composite is given. In addition, some technical informations in terms of the crack length by indentation in estimating the existence of the surface residual stress that prevents to obtain an accurate fracture toughness are presented.

• 대한기계학회논문집A
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• 제28권3호
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• pp.304-310
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• 2004

In this paper, cracking threshold for nanoindentation is analyzed by using 3D finited-element method. The analysis by maximum principal stress criterion can obtain the reliable results for determining to crack initiation location and load. Because the ratio of maximum principal stress to indentation depth for Victors indentation is smaller than flat-plane-column indentation and cracking for Victors indentation occurs from the inner part of specimen difficult to measure crack length, the nanoindentation facture test for flat-plane-column indentation is more effective.

• 한국세라믹학회지
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• 제24권4호
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• pp.313-320
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• 1987

Fracture toughness of hot pressed cordierite-SiC whisker ceramic composites contained up to 40vol.% SiC whiskers were determined by using the indentation crack length(IC), indentation strengthin-bending(IS), and single-edge notched-beam(SENB) methods. The results were compared to stress intensity factor, KB, at the crack branching boundary measured by using the mirror zone radius (MZ) method. IS method seems to provide a more reasonable estimation of fracture toughness than other methods for these composites.

• 한국세라믹학회지
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• 제34권8호
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• pp.877-885
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• 1997

The dependence of strength, crack growth, fracture mode and degree of domain rearrangement of PZT ceramics on poling strength were studied. The PZT [(Pb0.94Sr0.06)(Zr0.46Ti0.54)O3+Nb(trace)] specimens were poled at 0, 0.5, 1.0, 1.5, 2.0, 2.5, 3.0 kv/mm, and the strength of the specimens was measured by 3 point flexure system. The bending strength of the specimen decreased in different modes according to the bending directions; xz, zx and yz plane direction with x axis of the poling direction in Cartesian coordinate system. The strength differences between the directions increased as the poling strength increased. The fracture mode transferred to intergranular fracture mode from transgranular one as the poling strength increased. The mechanical breakdown occurred when the poling strength higher than 3 kV/mm was applied to the specimen. It was observed that the crack length increased in the normal direction to the poling direction, however, decreased in the parallel direction to the poling direction when the poled PZT specimen was indented by the Vickers indenter. However, the crack produced by indentation continuously was continuously increased little by little after indentation on the specimen. The domain rearrangement occurred as the poling strength increased and the domains were rearranged more effectively when the electric field was continuously increased little by little.

• 대한기계학회논문집A
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• 제26권10호
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• pp.2089-2095
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• 2002

Ceramic/metal composites have many attractive properties and great potential fur applications. Interfacial fracture properties of different layered composites are important in material integrity. Therefore, evaluation of fracture toughness at interface is required in essence. In this study, the mechanical characteristics for interface of ceramic/metal composites were investigated by indentation test of micro-hardness method. Apparent interfacial toughness of TBC system could be determined with a relation between the applied load and the length of the crack formed at the interface by indentation test.

• 한국세라믹학회지
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• 제38권5호
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• pp.454-460
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• 2001

장석, 석영, 점토와 17 wt% $Al_2$O$_3$를 함유한 알루미나질 자기 애자를 제조하였다. 분말을 ball milling으로 6시간 분쇄하였으며 성형체를 압출법으로 제조한 후 터널가마에서 130$0^{\circ}C$, 50분 동안 소결하였다. 터널가마에서 소결한 시편의 소결밀도는 이론밀도의 97%에 도달하였고, 3점 꺾임강도는 1658kgf/$ extrm{cm}^2$ 이었으며 ICL(indentation crack length) 방법으로 측정한 파괴인성은 2.3 MPa.m$^{1}$2/이었다. 기계적 성질을 향상시키기 위하여 ZrO$_2$를 첨가하여 15 wt% $Al_2$O$_3$-2 wt% ZrO$_2$와 12 wt% $Al_2$O$_3$-5 wt% ZrO$_2$를 복합체를 제조하였다. ZrO$_2$를 첨가한 시편의 꺾임강도는 1740kgf/$\textrm{cm}^2$이고 파괴인성은 2.4 MPa.m$^{1}$2/로 약 10% 기계적 성질이 향상되었다.

• The Korean Journal of Ceramics
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• 제1권4호
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• pp.197-203
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• 1995

Nearly fully dense PZT samples both with tetragonal and with morphotropic phase boundary compositions were prepared by the conventional powder processing and sintering. A micro-indentation technique was used to evaluate the dependence of fracture toughness on remanent polarization, crack length and the direction of crack propagation. The result shows that the toughness increases with the remanent polarization along the poling direction and decreases in the transverse direction. The dependence of toughness on the remanent polarization is neither symmetric nor linear but rather shown to be saturated quickly with the increase in remanent polariztion. R-curve behaviors are observed in both poled and unpoled samples. Sequential SEM and XRD studies on annealed, poled, ground, fractured and etched samples show that domain switching is evident as a viable toughening mechanism but might depend upon the rate of crack propagation. Grain bridging is also observed as one of the active toughening mechanisms.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 춘계학술대회논문집A
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• pp.121-126
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• 2000

Metal/Ceramic structures have many attractive properties, with great potential for applications that demand high stiffness, as well as chemical and biological stability, thermal and electrical insulation. They are currently in use for mechanical and thermal protection in cutting tool and engine parts. With all their great advantage, ceramics suffer from one major problem they are brittle, and are especially susceptible to cracking from surface contacts. Delamination at the interfaces with adjacent layers is a particularly disturbing problem, and can cause premature failure of a composite system. so determination of adhesive properties of coating is one of the most important problems for the extension of the use of coated materials. In this work, mechanical characteristics of Interface of ceramic/Metal composites are evaluated by means of hardness test, indentation test apparent interfacial toughness and bonding strength test. The interface indentation test provides a relation between the applied load(P) and the length of the crack(a) created at the interface between the coating and the substrate.