• Title/Summary/Keyword: Material Characterization

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Virtual Experimental Characterization of 3D Orthogonal Woven Composite Materials (직교 직물 복합재료 물성치 예측을 위한 가상 수치 실험)

  • Lee, Chang-Sung;Shin, Hun;Kim, Seung-Jo
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2001.05a
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    • pp.205-210
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    • 2001
  • In this work, virtual material characterization of 3D orthogonal woven composites is performed to predict the elastic properties by a full scale FEA. To model the complex geometry of 3D orthogonal woven composites, an accurate unit structure is first prepared. The unit structure includes warp yarns, filler yarns, stuffer yams and resin regions and reveals the geometrical characteristics. For this virtual experiments by using finite element analysis, parallel multifrontal solver is utilized and the computed elastic properties are compared to available experimental results and the other analytical results. It is founded that a good agreement between material properties obtained from virtual characterization and experimental results. Using the method of this virtual material characterization, the effects of inconsistent filler yarn distribution on the in-plane shear modulus and filler yarn waviness on the transverse Young's modulus are investigated. Especially, the stiffness knockdown of 3D woven composite structures is simulated by virtual characterization. Considering these results, the virtual material characterization of composite materials can be used for designing the 3D complex composite structures and may supplement the actual experiments.

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Issues with the electrical characterization of graphene devices

  • Lee, Byoung-Hun;Lee, Young-Gon;Jung, Uk-Jin;Kim, Yong-Hun;Hwang, Hyeon-Jun;Kim, Jin-Ju;Kang, Chang-Goo
    • Carbon letters
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    • v.13 no.1
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    • pp.23-28
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    • 2012
  • Graphene is an attractive material for device applications, but device characteristics are very unstable because the graphene is very sensitive to environmental factors such as charges nearby the graphene, metal contacts, defects, contaminants and other adsorbates. Since the interactions between graphene and environmental factors affect the electrical characteristics of graphene devices, the interpretation of electrical characteristics as simple as current-voltage curves is non-trivial, despite the common practice of using well known electrical characterization methods that have been used in silicon MOSFET. This paper addresses major obstacles in the electrical characterization of graphene devices and offers countermeasures to improve the accuracy of electrical characterization methods.

Proposal of a prototype plant based on the exfoliation process for the treatment of irradiated graphite

  • Pozzetto, Silvia;Capone, Mauro;Cherubini, Nadia;Cozzella, Maria Letizia;Dodaro, Alessandro;Guidi, Giambattista
    • Nuclear Engineering and Technology
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    • v.52 no.4
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    • pp.797-801
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    • 2020
  • Most of irradiated graphite that should be disposed comes from moderators and reflectors of nuclear power plants. The quantity of irradiated graphite could be higher in the future if high-temperature reactors (HTRs) will be deployed. In this case noteworthy quantities of fuel pebbles containing semi-graphitic carbonaceous material should be added to the already existing 250,000 tons of irradiated graphite. Industry graphite is largely used in industrial applications for its high thermal and electrical conductivity and thermal and chemical resistance, making it a valuable material. Irradiated graphite constitutes a waste management challenge owing to the presence of long-lived radionuclides, such as 14C and 36Cl. In the ENEA Nuclear Material Characterization Laboratory it has been successfully designed a procedure based on the exfoliation process organic solvent assisted, with the purpose of investigate the possibility of achieving graphite significantly less toxic that could be recycled for other purpose [1]. The objective of this paper is to evaluate the possibility of the scalability from laboratory to industrial dimensions of the exfoliation process and provide the prototype of a chemical plant for the treatment of irradiated graphite.

A Study on the Antibacterial Properties of Ag Electropulsed Anodized Aluminium Alloy (Pulse도금법에 의한 Ag주입 양극산화 알루미늄 합금의 항균특성에 관한 기초연구)

  • Lim, Ki-Young;Ki, Joon-Seo;Jang, Yong-Seok;Lee, Woo-Min;Yoon, Jeong-Mo
    • Korean Journal of Materials Research
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    • v.16 no.10
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    • pp.639-646
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    • 2006
  • Over the last two decades, microbiologically influenced corrosion (MIC) of metallic materials has received considerable attention due to its serious effects on industrial field. In this context, it is important to devise control methods which inhibit biofilm formation on various metallic compounds and are compatible with environment. It was change of various conditions (duty cycle, current density, $AgNO_3$ concentration and pH) for injection of Ag particles in anodized Aluminum alloy pore using pulsed current. Optimal condition was obtained by means of FE-SEM, ICP analysis etc. The antibacterial metal's specimen were manufactured under optimal condition and this specimen were tested the antibacterial characterization and anticorrosion characterization. In result of test, we can confirmed that the antibacterial characterization and anticorrosion characterization of the specimens of injected Ag particles in anodized Aluminum alloy pore using pulsed current were better than the anodized Aluminum alloy specimens.

A Study on Material Characterization of Semi-Solid Materials(II) -Determination of Flow Stress For Semi-Solid Materials Using Backward Extrusion Experiment with Model Material and Upper Bound Analysis- (반용융 재료의 물성치 평가에 관한 연구(II) -모델재료의 후방압출 실험과 상계해석을 통한 반용융 재료의 유동응력식 결정-)

  • 이주영;김낙수
    • Transactions of Materials Processing
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    • v.8 no.4
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    • pp.374-383
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    • 1999
  • To determine the flow stress of semi-solid materials, a new combined method has been studied by experimental and analytic technique in the current approach. Using backward extrusion experiment and its numerical analysis, the characterization scheme of semi-solid materials according to the change of initial solid volume fraction has been proposed. Because that solid volume fraction is sensitive to temperature change, it is required to precisely control the temperature setting. Model materials can guarantee the establishment of material characterization technique from the noise due to temperature change. Thus, clay mixed with bonded abrasives was used for experiment and the change of initial solid fraction was copied out through the variation of mixing ratio. Upper bound method was adapted to increase in efficiency of the calculation in numerical analysis and new kinematically admissible velocity field was employed to improve the accuracy of numerical solution. It is thought that the material characterization scheme proposed in this study can be applied to not only semi-solid materials, but also other materials that is difficult to obtain the simple stress state.

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The exfoliation of irradiated nuclear graphite by treatment with organic solvent: A proposal for its recycling

  • Capone, Mauro;Cherubini, Nadia;Cozzella, Maria Letizia;Dodaro, Alessandro;Guarcini, Tiziana
    • Nuclear Engineering and Technology
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    • v.51 no.4
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    • pp.1037-1040
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    • 2019
  • For the past 50 years, graphite has been widely used as a moderator, reflector and fuel matrix in different kinds of gas-cooled reactors. Resulting in approximately 250,000 metric tons of irradiated graphite waste. One of the most significant long-lived radioisotope from graphite reactors is carbon-14 ($^{14}C$) with a half-life of 5730 years, this makes it a huge concern for deep geologic disposal of nuclear graphite (NG). Considering the lifecycle of NG a number of waste management options have been developed, mainly focused on the achievement the radiological requirements for disposal. The existing approaches for recycling depend on the cost to be economically viable. In this new study, an affordable process to remove $^{14}C$ has been proposed using samples taken from the Nuclear Power Plant in Latina (Italy) which have been used to investigate the capability of organic and inorganic solvents in removing $^{14}C$ from exfoliated nuclear graphite, with the aim to design a practicable approach to obtain graphite for recycling or/and safety disposed as L& LLW.

A Study on Material Characterization of SMC (SMC의 물성치 평가에 관한 연구)

  • 정진호;한영원;임용택
    • Transactions of Materials Processing
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    • v.4 no.3
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    • pp.245-256
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    • 1995
  • SMC(Sheet Molding Compound), a thermoset composite material which consists of unsaturated polyester resin, fiberglass strands, fillers, and various chemical additives for curing agent, has been widely used in fabrication of structural components. The mechanical properties of molded SMS parts are strongly dependent on material flow results during compression molding process, while such flow in molds is affected by material characteristics. For numerical simulation of SMC molding process, estimation of material property of SMC must be accomplished. In this study, flow resistance of SMC was estimated through a simple compression test using a lubricant with grease oil under the constant strain rate condition at various temperatures and the result was compared with other material data available in the literature. The accuracy of the experimentally determined flow resistance was tested by finite element analyses of compression molding of SMC. Simulation results were compared with experimental results under the plane strain condition.

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Material Properties Characterization Based on Measurements of Reflection Coefficient and Bandwidth

  • Nguyen, Phuong Minh;Chung, Jae-Young
    • Journal of electromagnetic engineering and science
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    • v.14 no.4
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    • pp.382-386
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    • 2014
  • The knowledge of substrate material properties is important in antenna design. We present a technique to accurately characterize the dielectric constant and loss tangent of an antenna substrate based on the measurements of antenna's reflection coefficient and bandwidth. In this technique, an error function is formulated by combinations of the reflection coefficient and bandwidth of measured and simulated data, and then an optimization technique is used to efficiently search for the substrate properties that minimize the error function. The results show that the method is effective in retrieving the dielectric constant and loss tangent of the antenna substrate without the need of additional test fixtures as in conventional substrate characterization methods.

Characterization of Field-Aged Polymer Insulators for Distribution Power Systems (배전용 폴리머애자의 현장열화 특성평가)

  • 이병성;김찬영;한재홍
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.13 no.10
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    • pp.847-858
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    • 2000
  • The aging characteristics of 2 kinds of 3 years field-aged distribution polymer insulators which were dismounted from 5 regions have been investigated by electrical test and material characterization. Although the tan $\delta$of specimens prepared from weathershed was increased with surface aging, the tan $\delta$and leakage current of real products had no difference between virgin and dismounted ones. Due to the aging, all dismounted polymer insulators had micro-cracks on the surface of weathershed and only the products of manufacturer B showed the reduction of OIT(oxidation induction time). But, there were no differences between virgin and dismounted products in contact angle and chemical structure. Therefore, it can be considered that the aging is only limited on the surface of dismounted polymer insulators and that NMR technique are very useful to evaluate the aging of polymer materials.

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