• Title/Summary/Keyword: Pore control fiber

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Characterization of nano-fiber web structures using a morphological image processing

  • Kim, Jooyong;Lee, Jung-Hae
    • Proceedings of the Korean Fiber Society Conference
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    • 2003.10a
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    • pp.100-100
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    • 2003
  • An image processing algorithm has been developed in order to analyze the nanofiber web images obtained from a high magnification microscope. It has been known that precise pore detection on thick webs is extremely difficult mainly due to lack of light uniformity, difficulty of fine focusing and translucency of nanofiber web. The pore detection algorithm developed has been found to show excellent performance in characterizing the porous structure, thus being a promising tool for on-line quality control system under mass production. Since the images obtained from an optical microscope represent only web surface, a scale factor has been introduced to estimate the web structure as a whole. Resulting web structures have been compared to those by mercury porosimetry, especially in pore size distribution. It has been shown that those two structures have a strong correlation, indicating that scaling of a single layer web structure can be an effective way of estimating the structure of thick fiber webs.

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On-line Measurement and Characterization of Nano-web Qualities Using a Stochastic Sensor Fusion System Design and Implementation of NAFIS(NAno-Fiber Information System)

  • Kim, Joovong;Lim, Dae-Young;Byun, Sung-Weon
    • Proceedings of the Korean Fiber Society Conference
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    • 2003.10a
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    • pp.45-46
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    • 2003
  • A process control system has been developed for measurement and characterization of the nanofiber web qualities. The nano-fiber information system (NAFIS) developed consists of a measurement device and an analysis algorithm, which are a microscope-laser sensor fusion system and a process information system, respectively. It has been found that NAFIS is so successful in detecting irregularities of pore and diameter that the resulting product has been quitely under control even at the high production rate. Pore distribution, fiber diameter and mass uniformity have been readily measured and analyzed by integrating the non-contact measurement technology and the random function-based time domain signal/image processing algorithm. Qualifies of the nano-fiber webs have been revealed in a way that the statistical parameters for the characteristics above are calculated and stored in a certain interval along with the time-specific information. Quality matrix, scale of homogeneity is easily obtained through the easy-to-use GUI information. Finally, ANFIS has been evaluated both for the real-time measurement and analysis, and for the process monitoring.

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Usable water production from coal seam gas water with a combination of pore control fiber filtration and reverse osmosis

  • Shin, Choon Hwan;Bae, Jun Seok
    • Environmental Engineering Research
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    • v.23 no.2
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    • pp.210-215
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    • 2018
  • Coal seam gas (CSG) water, to be discharged, has been usually treated in reverse osmosis (RO) plants which require extensive and expensive pre-treatment. However, current low gas prices have been a great driver for relevant industries to seek for alternative cost-effective technologies in the aspect of its beneficial use and fit-for-purpose usable water production. In this paper, a combined system with a two-stage pore control fiber (PCF) filtration and a RO system was designed and tested for CSG water treatment. Also, a coagulation reactor was placed in front of the PCF to further enhance suspended solid removal. More than 99% of SS were removed through the PCF filtration while organic, total nitrogen and total phosphorous were mostly removed by the RO system. Especially along with a decrease in conductivity, the total dissolved solid derived from salts was mainly removed in the RO system. Having $OH^-$ undetected, $HCO_3{^-}$ was found to be a dominant compound and its removal efficiency was 97-98% after the RO treatment. And a Fe(III) type of Polytetsu, which was the first to be tested in this paper, was found to be a better option than a Al(III) type of Poly Aluminium Chloride due to its greater coagulation efficiency and applicability at a broader range of pH than the Al(III) type. In addition, there was no noticeable change in oxidation reduction potential, suggesting that an additional process is required to oxidize non-ionic organic carbons (detected as total organic carbon).

Structure Variation of Polypropylene Hollow Fiber Membrane with Operation Parameters in Stretching Process (연신 공정 조업변수에 따른 폴리프로필렌 중공사막의 구조 변화)

  • Lee Gyu-Ho;Kim Jin-Ho;Song Ki-Gook;Kim Sung-Soo
    • Polymer(Korea)
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    • v.30 no.2
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    • pp.175-181
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    • 2006
  • Hybrid process of thermally-induced phase separation and stretching was developed for the preparation of microporous polypropylene hollow fiber membranes. Precursor for stretching was prepared by using soybean oil as a diluent and benzoic acid as a nucleating agent far the sphenlite control and it was stretched far the micrporous hollow fiber membrane. The effects of stretching ratio and deformation rate for stretching process were investigated. Increase of stretching ratio resulted in the greater pore size with nonuniform size distribution. Higher deformation rate also increaser the pore size with uniform size distribution. Stretching ratio was closely related with the orientation of polymer chain and increased the mechanical strength of the fiber. Increase of deformation rate had little effects on the orientation of crystalline phase, and decreased the orientation of amorphous phase which caused the decrease of tensile strength of the fiber and broke the micro-fibrils connecting spherulites to form a circular pore shape.

Pore Structure Characterization of Poly(vinylidene chloride)-Derived Nanoporous Carbons

  • Jung, Hwan Jung;Kim, Yong-Jung;Lee, Dae Ho;Han, Jong Hun;Yang, Kap Seung;Yang, Cheol-Min
    • Carbon letters
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    • v.13 no.4
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    • pp.236-242
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    • 2012
  • Poly(vinylidene chloride) (PVDC)-derived nanoporous carbons were prepared by various activation methods: heat-treatment under an inert atmosphere, steam activation, and potassium hydroxide (KOH) activation at 873, 1073, and 1273 K. The pore structures of PVDC-derived nanoporous carbons were characterized by the $N_2$ adsorption technique at 77 K. Heat treatment in an inert atmosphere increased the specific surface area and micropore volume with elevating temperature, while the average micropore width near 0.65 nm was not significantly changed, reflecting the characteristic pore structure of ultramicroporous carbon. Steam activation for PVDC at 873 and 1073 K also yielded ultramicroporosity. On the other hand, the steam activated sample at 1273 K had a wider average micropore width of 1.48 nm, correlating with a supermicropore. The KOH activation increased the micropore volume with elevating temperature, which is accompanied by enlargement of the average micropore width from 0.67 to 1.12 nm. The average pore widths of KOH-activated samples were strongly governed by the activation temperature. We expect that these approaches can be utilized to simply control the porosity of PVDC-derived nanoporous carbons.

The Compressive Strength and Durability Properties of Polypropylene Fiber Reinforced EVA Concrete (폴리프로필렌 섬유 보강 EVA 콘크리트의 압축강도 및 내구성)

  • Nam, Ki Sung;Sung, Chan Yong
    • Journal of The Korean Society of Agricultural Engineers
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    • v.57 no.4
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    • pp.11-19
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    • 2015
  • The important properties of EVA (ethylene vinyl acetate) redispersible polymer was waterproof, densification of internal pore space of concrete and ball bearing and micro filler. Also, the significant role of polypropylene(PP) fiber was crack control and blockade of movement for deterioration factors. The most studies for EVA were limited in the field of mortar and PP fiber reinforced concrete had been studied in the state of being restricted unit water content, rich mix and mixing much of the fiber without considering construction site. Therefore, the control mix design were applied in ready mixed concrete using 10 % fly ash of total cement weight used in batch plant. On the basis of control mix design, EVA contents ranging from 0 % to 10 % of total cement weight and PP fiber contents ranging from 0 % to 0.5 % of EVA concrete volume were used in the mix designs. The results showed the maximum compressive strength value was measured at EVA 5.0 % and PP fiber 0.1 %, the minimum water absorption ratio was at EVA 10 % and PP fiber 0 %, the durability factor for freezing and thawing resistance was at EVA 5.0 % and PP fiber 0.3 % and the minimum weight reduction ratio of resistance to sulfuric acid attack was at EVA 10 % and PP fiber 0.5 % after curing age 42days. Meanwhile, From these results, PP fiber reinforced EVA concrete would be very benefit, if each optimal mix types were used in hydraulic structures, underground utilities and agricultural structures.

Effect of High-Temperature Spinning and PVP Additive on the Properties of PVDF Hollow Fiber Membranes for Microfiltration

  • Cha, Bong-Jun;Yang, Jung-Mok
    • Macromolecular Research
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    • v.14 no.6
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    • pp.596-602
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    • 2006
  • The effect of high-temperature spinning and poly(vinyl pyrrolidone) (PVP) additive on poly(vinylidene fluoride) (PVDF) hollow fiber membranes was investigated using differential scanning calorimetry, X-ray diffraction measurement, and scanning electron microscopy, together with the corresponding microfiltration performances such as water flux, rejection rate, and elongational strength. Using high-temperature spinning, porous hollow fiber membranes with particulate morphology were prepared through PVDF crystallization. The particulate structure of the membranes was further modified by the addition of miscible PVP with PVDF. Due to these effects, the rejection rate and strength of the fibers were increased at the expense of reduced water flux and mean pore size, which indicates that high-temperature spinning and PVP addition are vary effective to control the morphology of PVDF hollow fiber membranes for microfiltration.

Effects of Surfactants on Dispersion Behavior of Vectran® in Water(II) -Study on the Manufacture and Properties of Wet-laid Nonwoven Fabrics- (Vectran®의 수중 분산 거동에 미치는 계면활성제의 영향(II) - 습식부직포의 제조와 그 물성연구 -)

  • Kang, Yoo-Jung;Song, Sun-Hye
    • Textile Coloration and Finishing
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    • v.27 no.4
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    • pp.327-333
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    • 2015
  • This paper aims to manufacture nonwoven fabrics by wet-laid technology using Vectran$^{(R)}$ one of the highly favoured high-performace fiber. In previous study, a novel evaluation on fiber dispersion was studied to select optimum surfactant by the need for the control of fiber dispersion in water with reference to wet-laid nonwoven technology. 3 Types of sulfonate anionic surfactants were chosen and added in a stage of agitation to improve dispersion behavior of fibers in water. It was observed that the state of fiber dispersion in water affected various properties of nonwovens, including appearance, physical properties, and mechanical properties. Nonwoven added SDBS was uniform in web structure, thickness and weight. Its average pore was small in size and consisted of fine pores and the value of porosity was high. Further, the difference of tensile value between 2 directions was the least. Consequentially, as the dispersion behavior of fiber increases, nonwoven shows more balanced and uniform physical properties in all directions.

Spalling Properties of High Strength Concrete Mixed with Various Mineral Admixtures Subjected to Fire

  • Han, Cheon-Goo;Han, Min-Cheol;Heo, Young-Sun
    • International Journal of Concrete Structures and Materials
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    • v.2 no.1
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    • pp.41-48
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    • 2008
  • This study investigates the spalling properties of high strength concrete designed with various types of mineral admixture and diverse content ratios of polypropylene (PP) fiber. Experimental factors considered in series I are four pozzolan types of mineral admixture and series II consists of three shrinkage reducing types of mineral admixture. PP fiber was added 0.05, 0.10 and 0.15vol. % in each mixture of series I and series II, so that totally 27 specimens including control concretes in each series were prepared. Test results showed that the increase of fiber content decreased the slump flow of fresh concrete and increased or decreased the air content depending on the declining ratio of slump flow. For the properties of compressive strength, all specimens were indicated at around 50 MPa, which is high strength range; especially all specimens in series II were 60 MPa. Fire test was conducted in standard heating curve of ISO 834 with ${\phi}100{\times}200\;mm$ size of cylinder moulds for 1 hour. The specimens incorporating silica fume exhibited severe spalling and most specimens without the silica fume could be protected from the spalling occurrence in only 0.05vol % of PP fiber content. This fire test results demonstrated that the spalling occurrence in high strength concrete was not only affected by concrete strength related to the porosity of microstructure but also, even more influenced by micro pore structure induced by the mineral admixtures.