• Title/Summary/Keyword: Solid composites

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Preparation and Evaluation of Solid Composites Containing Choline Alphoscerate

  • Kim, Hoon;Cho, Seong-Wan
    • Biomedical Science Letters
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    • v.25 no.2
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    • pp.170-176
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    • 2019
  • The objective of this study was to evaluate the characteristics of the mixtures of choline alphoscerate (alpha-glycerylphosphorylcholine, alpha-GPC), in the liquid form, and sucrose ester, which formed a solid composite. The choline alphoscerate solid composites were prepared using different ratios of sucrose ester, and different preparation methods, such as air drying and rotary evaporation, were compared for their preparation efficacy. We examined the characteristics of the solid composites by using scanning electron microscopy (SEM), angle of repose, and moisture content. The ideal mixing ratio of choline alphoscerate and sucrose ester was determined as 1:3 and air drying was found to be more suitable for the preparation of solid composites than rotary evaporation. SEM measurements of the degree of dispersion and the size of particles indicated that a high-temperature air method was more suitable. These results demonstrated the successful preparation of choline alphoscerate solid composites that have potential for industrial use.

Fatigue modeling of chopped strand mat/epoxy composites

  • Shokrieh, M.M.;Esmkhania, M.;Taheri-Behrooz, F.
    • Structural Engineering and Mechanics
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    • v.50 no.2
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    • pp.231-240
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    • 2014
  • In the present research, fatigue behavior of chopped strand mat/epoxy composites has been studied with two different techniques. First, the normalized stiffness degradation approach as a well-known model for unidirectional and laminated composites was utilized to predict the fatigue behavior of chopped strand mat/epoxy composites. Then, the capability of the fatigue damage accumulation model for chopped strand mat/epoxy composites was investigated. A series of tests has been performed at different stress levels to evaluate both models with the obtained results. The results of evaluation indicate a better correlation of the normalized stiffness degradation technique with experimental results in comparison with the fatigue damage accumulation model.

Flexural fatigue modeling of short fibers/epoxy composites

  • Shokrieh, M.M.;Haghighatkhah, A.R.;Esmkhani, M.
    • Structural Engineering and Mechanics
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    • v.64 no.3
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    • pp.287-292
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    • 2017
  • In the present research, an available flexural stiffness degradation model was modified and a new comprehensive model called "X-NFSD" was developed. The X-NFSD model is capable of predicting the flexural stiffness degradation of composite specimen at different states of stresses and at room temperature. The model was verified by means of different experimental data for chopped strand mat/epoxy composites under displacement controlled bending loading condition at different displacements and states of stresses. The obtained results provided by the present model are impressively in very good agreement with the experimental data and the mean value of error of 5.4% was achieved.

A Novel Route to Realise High Degree of Graphitization in Carbon-carbon Composites Derived from Hard Carbons

  • Mathur, R.B.;Bahl, O.P.;Dhami, T.L.;Chauhan, S.K.
    • Carbon letters
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    • v.4 no.3
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    • pp.111-116
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    • 2003
  • Carbon/carbon composites were developed using PAN based carbon fibres and phenolic resin as matrix in different volume fractions and heat treated to temperatures between $1000^{\circ}C$ to $2500^{\circ}C$. Although both the starting precursors are nongraphitizing hard carbons individually, their composites lead to very interesting properties e.g. x-ray diffractograms show the development of graphitic phase for composites having fibre volume fractions of 30~40%. Consequently the electrical resistivity of such composites reaches a value of $0.8\;m{\Omega}cm$, very close to highly graphitic material. However, it was found that by increasing the fibre volume fraction to 50~60%, the trend is reversed. Optical microscopy of the composites also reveals the development of strong columnar type microstructure at the fibre (matrix interface due to stress graphitization of the matrix. The study forcasts a unique possibility of producing high thermal conductivity carbon/carbon composites starting with carbon fibres in the chopped form only.

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The effect of nanoparticles on enhancement of the specific mechanical properties of the composite structures: A review research

  • Arani, Ali Ghorbanpour;Farazin, Ashkan;Mohammadimehr, Mehdi
    • Advances in nano research
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    • v.10 no.4
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    • pp.327-337
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    • 2021
  • In this review, composite structures are used for many industries for at least four decades. Polymeric composites are one of the important structures in the aerospace and aviation industry because of their high strength and low weight. In this comprehensive review, mechanical behaviors, physical and mechanical properties of polymeric composites, different types of reinforcements, different methods to fabricate polymeric composites, historical structural composite materials for aviation and aerospace industries, and also different methods for the characterization are reported. How to use various methods of composite preparation using different nanofillers as reinforcements and its effect on the physical properties and mechanical behavior of composites are discussed as well.

Fabrication of Metal Matrix Composites and Development of Forming System in Mashy State (반응고법에 의한 금속복합재료의 제조 및 성형 시스템의 개발)

  • 강충길;김현우;김영도
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.14 no.3
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    • pp.581-593
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    • 1990
  • A semi-solid alloy in which solid and liquid phase are co-existing is obtained by strirring of Al7075 molten metal. A semi-solid alloy is dependent on the corresponding temperature within the solid-liquid range, and the process parameters should be controlled accurately to obtain the homogeneous semi-solid alloy. The possibility o homogeneous fiber-reinforce aluminum alloy by addition of $Al_{2}$O$_{3}$ short fibers with vigorous agitation was investigated. The billet of composite materials was fabricated by squeeze casting, and homogeneous dipersion state of fibers in billet of fabricated metal matrix composites was observed. A slurry of semi-solid short fiber metal matrix composites is used in the direct rolling process, and this process showed the fabrication possibility of metal matrix composite sheets. The fabricated sheet was tested regarding vickers hardness, elongation and micro-structure. It has become clear that mashy state processing and working are very useful to obtain parts of composites material closed to near net shape.

Effects of Orientation via Solid-State Extrusion on Properties of Polypropylene/Mica Composites (폴리프로필렌/마이카 복합재료의 물성에 미치는 고상압출 배향의 영향)

  • Lee, Jae Choon;Ha, Chang-Sik
    • Journal of Adhesion and Interface
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    • v.15 no.1
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    • pp.9-13
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    • 2014
  • The purpose of this work is to investigate the specific gravity, thermal, and mechanical property changes of polypropylene (PP)/mica composites before and after solid-state extrusion. On increasing the filler content, the specific gravity of the composites increased. The specific gravity of the oriented specimen containing filler in PP matrix is found to be much smaller than that of pre-specimen due to the formation of more microvoids. The presence of microvoids in the case of oriented composite specimen significantly affected the tensile and flexural properties of the composites. Both flexural strength and modulus of the composites showed maxima when the mica contents was 10 wt%, regardless of the orientation via solid state extrusion.

Preparation and Thermal Performance of Fullerene-Based Lead Salt

  • Guan, Hui-Juan;Peng, Ru-Fang;Jin, Bo;Liang, Hua;Zhao, Feng-Qi;Bu, Xing-Bing;Han, Wen-Jing;Chu, Shi-Jin
    • Bulletin of the Korean Chemical Society
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    • v.35 no.8
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    • pp.2257-2262
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    • 2014
  • $C_{60}$ is widely investigated because of its unique structure. But its applications in solid propellant seem to be relatively neglected. $C_{60}$ has more outstanding features than carbon black which is widely used as a catalyst ingredient of solid propellant. To combine the advantages of fullerene and lead salts, another good composite in propellant catalysts, we synthesized a kind of fullerene phenylalanine lead salt (FPL) and explored its thermal performances by differential thermal analysis (DTA) and thermogravimetry analysis (TGA). The results show it undergoes four exothermic processes started from 408 K. Combined TGA and X-ray diffractometer (XRD), the decomposition mechanism of FPL was derived by TG-IR and comparing IR spectra of FPL and its residues after burned to $327^{\circ}C$, $376^{\circ}C$ and $424^{\circ}C$, respectively. Effect of FPL on the decomposition characteristic of hexogen (RDX), a type of explosive in propellant, has been investigated using DTA at different heating rate, which shows the decomposition temperatures of the explosive are all reduced by more than 20 K. The corresponding activation energy ($E_a$) is decreased by $30kJ{\cdot}mol^{-1}$. So FPL has potential application as a combustion catalyst in solid propellant.

Wear Characterization of $Al/Al_2O_3$ Composites Reinforced with Hybrid of Carbon Fibers and SiC Whiskers (탄소섬유와 SiC 휘스커를 혼합한 $Al/Al_2O_3$ 복합재료의 마멸특성)

  • 봉하동;송정일;한경섭
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.19 no.7
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    • pp.1619-1629
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    • 1995
  • The Al/Al$_{2}$O$_{3}$ SiC and Al/Al$_{2}$O$_{3}$/C hybrid metal matrix composites (MMCs) were fabricated by squeeze infiltration method. Uniform distribution of reinforcements were found in the microstructure of metal matrix composites. Mechanical tests were carried out under various test conditions to clearly identify mechanical behavior of MMCs, and the wear mechanism of Al/Al$_{2}$O$_{3}$/(SiC or C) hybrid metal matrix composites were investigated. The tensile strength and hardness of hybrid composites was resulted in increasing compared with those of the unreinforced matrix alloy. Wear resistance was strongly dependent upon kinds of fiber, volume fraction and sliding speed. The wear resistance of metal matrix composites was remarkably improved by the addition of reinforcements. Especially, the wear resistance of the hybrid composites of carbon fibers was more effective than in the composites reinforced with alumina and SiC whiskers of reinforcements. This was due to the effect of carbon fiber on the solid lubrication. Wear mechanisms of hybrid composites were suggested from wear surface analyses. The major wear mechanism of hybrid composites was the abrasive wear at low to intermediate sliding speed, and the melting wear at intermediate to high sliding speed.

Solid State Sintering of Calcium Phosphate Ceramic Composites and Their Cellular Response

  • Cho, Yeong-Cheol;Kong, Young-Min;Riu, Doh-Hyung
    • Korean Journal of Metals and Materials
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    • v.50 no.9
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    • pp.691-695
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    • 2012
  • Calcium phosphate ceramic composites, consisting of hydroxyapatite(HA) and tricalcium phosphate (TCP), were fabricated by solid state sintering in order to investigate the effect of their initial compositions on microstructural evolutions and biocompatibility. All the sintered calcium phosphate ceramics exhibited almost full densification, while the grain growth of the composites increased with an increasing TCP content in the green body. The TCP phase transformed into a Ca-deficient HA phase during sintering via the diffusion of calcium ions from the HA phase into the TCP phase. The phases formed in the composites significantly affected the biocompatibility of the composites. The HA-matrix ceramic composites with TCP had a better cellular response than the pure HA ceramics, presumably due to the newly formed Ca-deficient HA.