• Title/Summary/Keyword: Standard uncertainty

Search Result 638, Processing Time 0.025 seconds

A Study on the Measurement Uncertainty of Flowmeter Calibrator (유량계 교정장치의 측정불확도에 관한 연구)

  • Im, Gi-Won
    • Transactions of the Korean Society of Mechanical Engineers B
    • /
    • v.25 no.4
    • /
    • pp.561-571
    • /
    • 2001
  • The standard uncertainty of flowrate measurement is obtained by combining that of independent variables. Gravimetric and volumetric method were applied to determine the flowrate and the standard uncertainties of flowrate measurement by both methods were evaluated in accordance with the procedure recommended by International Organization for Standardization. The combined standard uncertainties of determining the flowrate were estimated from the sensitivity coefficient and the standard uncertainty of independent variables. For practical application, the methods for evaluating and expressing uncertainty in flow measurement were discussed. It was found that the uncertainties of the weighing and time measurement in gravimetric method, the volume and time measurement in volumetric method have dominant influence on that of flowrate measurement. With the quantitative analysis of the sensitivity coefficient, the contribution of the each variable uncertainty to the combined standard uncertainty of flowrate measurement is shown clearly.

Uncertainty in Determination of Menthol from Mentholated Cigarette (담배 중 멘톨 분석에 대한 불확도 측정)

  • 장기철;이운철;백순옥;한상빈
    • Journal of the Korean Society of Tobacco Science
    • /
    • v.22 no.1
    • /
    • pp.91-98
    • /
    • 2000
  • This study was carried out to evaluate the uncertainty in the analysis of menthol content from the mentholated cigarette. Menthol in the sample cigarette was extracted with methanol containing an anethole as an internal standard, and then analyzed by gas chromatography. As the sources of uncertainty associated with the analysis of menthol, were the following points tested, such as the weighing of sample, the preparation of extracting solution, the pipetting of extracting solution into the sample, the preparation of standard solution, the precision of GC injections for standard & sample solution, the GC response factor of standard solution, the reproducibility of menthol analysis, and the determination of water content in tobacco, etc. For calculating the uncertainties, type A of uncertainty was evaluated by the statistical analysis of a series of observation, and type B by the information based on supplier's catalogue and/or certificated of calibration. Sources of uncertainty were subsequently included and mathematically combined with the uncertainty arising from the assessment of accuracy to provide the overall uncertainty. It was shown that the main source of uncertainty came from the errors in the reproducibility of menthol and water determination, the purity of menthol reference material in the preparation of standard solution, and the precision of GC injections for sample solution. The errors in sample weighing and volume measurement contributed relatively little to the overall uncertainty. The expanded uncertainty in the mentholated cigarettes, Korean and American brand, at 0.95 level of statistical confidence was $\pm$0.06 and $\pm$0.07 mg/g for a menthol content of 1.89 and 2.32 mg/g, respectively.

  • PDF

A Study on the Development and the Uncertainty Analysis of Oil Flow Standard System (기름 유량표준장치의 개발 및 측정 불확도에 관한 연구)

  • Lim, Ki-Won;Choi, Jong-Oh
    • Transactions of the Korean Society of Mechanical Engineers B
    • /
    • v.27 no.8
    • /
    • pp.1071-1080
    • /
    • 2003
  • A national standard system was developed in order to calibrate and test the oil flowmeters for the petroleum field. A stop valve and a gyroscopic weighing scale were employed for the primary standard of the flow quantity. It is operated by the standing start and finish mode and the static weighing method. The model equation for uncertainty evaluation was based on the calibration principle of standard system. The sources of the uncertainties were quantified and combined according to the GUM(Guide to the Expression of Uncertainty in Measurement). It was found that the standard system had the relative expanded uncertainty of 0.04 % in the range of 18 - 350 ㎥/h. According to the uncertainty budget, the uncertainties of the fluid density and the volume of pipeline, which were temperature dependent, contributed 92% of final uncertainty in the oil flow standard system.

Uncertainty of Measurement in Nitrate Analysis from Burley Leaf Tobacco (버어리종 담배 중 질산성 질소에 대한 측정불확도)

  • Lee Jeong-Min;Lee Kyoung-Ku;Han Sang-Bin
    • Journal of the Korean Society of Tobacco Science
    • /
    • v.27 no.2
    • /
    • pp.226-234
    • /
    • 2005
  • The uncertainty of measurement in nitrate from burley leaf tobacco by continuous-flow analysis method was evaluated following internationally accepted guidelines. The sources of uncertainty associated with the analysis of nitrate were weight of standard and sample, purity of standard, dilution of standard solution, calibration curve, water content, etc. The calculation of uncertainty based on the GUM(Guide to the Expression of Uncertainty in Measurement) and EURACHEM/CITAC Guide. An expanded uncertainty was obtained by multiplying the combined standard uncertainty with a coverage factor (k) calculated from the effective degree of freedom. The concentration of nitrate from burley leaf tobacco was $2.09\%$ and the expanded uncertainty by multiplying by the coverage factor(k, 2.20) was $0.13\%\;at\;a\;95\%$ confidence level.

Model Classification and Evaluation of Measurement Uncertainty (측정 불확도 모형 분류 및 평가)

  • Choi, Sung-Woon
    • Journal of the Korea Safety Management & Science
    • /
    • v.9 no.1
    • /
    • pp.145-156
    • /
    • 2007
  • This paper is to propose model classification and evaluation of measurement uncertainty. In order to obtain type A and B uncertainty, variety of measurement mathematical models are illustrated by example. The four steps to evaluate expanded uncertainty are indicated as following; First, to get type A standard uncertainty, measurement mathematical models of single, double, multiple, design of experiment and serial autocorrelation are shown. Second, to solve type B standard uncertainty measurement mathematical models of empirical probability distributions and multivariate are presented. Third, type A and B combined uncertainty, considering sensitivity coefficient, linearity and correlation are discussed. Lastly, expanded uncertainty, considering degree of freedom for type A, B uncertainty and coverage factor are presented with uncertainty budget. SPC control chart to control expanded uncertainty is shown.

Uncertainty Analysis of Cross-Correlation Algorithm based on FFT by PIV Standard Images (표준 영상에 의한 FFT 기반 상호상관 PIV 알고리즘의 불확도 해석)

  • Lee, Suk-Jong;Choi, Jung-Geun;Sung, Jae-Young;Hwang, Tae-Gyu;Doh, Deog-Hee
    • Journal of the Korean Society of Visualization
    • /
    • v.3 no.2
    • /
    • pp.71-78
    • /
    • 2005
  • Uncertainty introduced by a cross-correlation algorithm based on FFT has been investigated using PIV standard images. The standard images were generated by the Monte Carlo simulation method. Both bias and random errors from the velocity vector have been analyzed with regard to the particle diameter, displacement, and the number of particles. The uncertainty of velocity is evaluated based upon the IS0/IEC standard. As a result, a total error of $0.26\%$ is included in the PIV cross-correlation algorithm. In addition, the uncertainty budget is presented, where the effect of the above three variables is examined. According to the budget, the variation of the number of particles within the interrogation window mainly contributes to the combined standard uncertainty of the real measured velocity field when excluding the effect of errors by the experiments itself. Finally, the expanded uncertainty is found to be about $12\%$ at the $95\%$ confidence level.

  • PDF

Application of the uncertainty for insertion loss measurement of silencers (소음기 감음 성능 불확도 산출 방법 연구)

  • Yu, Seung-Guk;Kim, Dae-Hyeon;Kim, Yeong-Chan;Kim, Du-Hun
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
    • /
    • 2000.06a
    • /
    • pp.1675-1680
    • /
    • 2000
  • Recently the uncertainty has been made rapid progress in various fields of industry but the uncertainty measurement method of acoustical test (i.e. Insertion loss, Absorption ratio, Transmission loss etc,) hasn't been established. In this study, the uncertainty of measurement method for ducted silencers is carried out according to ISO 7235. The standard uncertainty factors are composed of sound pressure level, microphone sensitivity and pistonphone calibration in this measurement. Sound pressure level is type A evaluation of uncertainty, microphone sensitivity and pistonphone calibration are type B evaluation of uncertainty. The combined standard uncertainty is calculated by two type evaluation. The expanded uncertainty is expressed by the combined standard uncertainty multiply k value which is yield the effective degree of freedom.

  • PDF

Long Term Stability of Uncertainty Analysis of Light Oil Elow Standard System (장기 안정성을 고려한 경질유 유량표준장치 불확도 평가)

  • Lim, Ki-Won;Choi, Jong-Oh
    • Transactions of the Korean Society of Mechanical Engineers B
    • /
    • v.29 no.10 s.241
    • /
    • pp.1130-1138
    • /
    • 2005
  • A national standard system for the petroleum field has been developed to calibrate and test the oil flow meters in Korea. The operating system and the uncertainty of the system were evaluated by the peer reviewers of foreign national metrology institutes in 2002. Since the characteristics of the system might be changed by time, the uncertainty of the system is reevaluated with the consideration of the long term stability of the system. It is found that the system has a relative expanded uncertainty of 0.048 $\%$ in the range of $15\~120\;m^3/h$. According to the uncertainty budget, the uncertainties of the fluid density and the final mass measurement, which are temperature dependent, contribute about $94\%$ of the total uncertainty in the oil flow standard system

Calibration uncertainty of a spinning rotor gauge (스피닝 로터 게이지 교정 불확도)

  • 홍승수;임인태;신용현;정광화
    • Journal of the Korean Vacuum Society
    • /
    • v.12 no.1
    • /
    • pp.7-15
    • /
    • 2003
  • Spinning Rotor Gauge (SRG) has been used to transfer standard gauge for international comparison at the high vacuum standards. We calibrated a spinning rotor gauge by using dynamic calibration system (DCS) that was a national high vacuum standards system. And its uncertainties were evaluated with the International Organization for Standardization (ISO), they were recognized ai A type uncertainty, B type uncertainty, combined Standard uncertainty, and expanded uncertainty. The combined standard uncertainties were $1.8007\times10^{-5}$ Pa ~ ~$4.8422\times10^{-5}$ Pa for this spinning rotor gauge.

Estimation of Measurement Uncertainty in Evaluation of Tensile Properties (인장 물성 측정 불확도 평가)

  • Huh, Y.H.;Lee, H.M.;Kim, D.J.;Park, J.S.
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • v.34 no.1
    • /
    • pp.73-78
    • /
    • 2010
  • Estimation of tensile properties measurement uncertainty of material was carried out. Sources of uncertainty affecting the measurement of tensile properties were classified and analyzed. The models for uncertainty evaluation of measurands to be determined from tensile test, such as elastic modulus, yield strength and tensile strength, were suggested and derived from the mathematical relations, corresponding to the respective measurands, and the measuring quantities by calculating each sensitivity coefficient of the quantities. Based on these models, the uncertainty of the tensile properties was evaluated from the experimental data of SUS316LN determined according to ISO 6892.