• Title/Summary/Keyword: aluminum compound

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RADIOLOGIC STUDY OF THE EXPERIMENTALLY PRODUCED BONE DESTRUCTION AND BONE FORMATION (실험적 골파괴와 골형성에 대한 방사선학적 연구)

  • Choi Soon-Chul;Ahn Hyung-Kyu
    • Journal of Korean Academy of Oral and Maxillofacial Radiology
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    • v.18 no.1
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    • pp.13-25
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    • 1988
  • Bone destruction was induced experimentally by the insertion of a bit of the arsenic compound into the pulp chambers of the right premolars and the artificial bone defects were produced in the periapical regions of the left premolars in 7 dogs. The serial standardized periapical radiographs using aluminum stepwedge attached to the XCP instruments, and resin bite blocks were taken following insertion of arsenic compound and at 2, 4, 7, 10, 14, 17, 21, 24 and 28 days in case of bone destruction and following bone injury and weekly thereafter for a total of 14 weeks in case of bone formation. The errors of the method were determined with error estimators described by the Duinkerke. All radiographs were evaluated by the visual examination after joint evaluation by three dental radiologists and analysed with densitometer. The following results were obtained; 1. Analysis of the bone destruction process 1) The error of the method in estimating two distances proved to be small (S.D. for the measuring error; 0.04㎜, S.D. for the over-all error; 0.06㎜, S.D. for the positioning error; 0.05㎜) 2) The radiographic changes were observed after 7 days in 6 cases, 4 days in 1 case and 10 days in 1 case by the visual examination. 3) Aluminum equivalent values were diminished after 2 days and the diminution of 0.58±0.19㎜ was demanded to be detected by the visual examination. 2. Analysis of the bone formation process 1) The error of the method in estimating two distances proved to be small (S.D. for the measuring error; 0.03㎜, S.D. for the over-all error; 0.04㎜ S.D. for the positioning error; 0.04㎜) 2) The radiographic changes were observed after 2 weeks in 5 cases and 3 weeks in 2 cases by the visual examination. 3) Aluminum equivalent values were increased after 1 week and the increase of 0.45±0.15㎜ was demanded to be detected by the visual examination. 4) Aluminum equivalent values were increased continuously for 7 or 9 weeks but there as only extremely small change after 10 weeks.

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Hardening Characteristics of Aluminum Alloy Surface by PTA Overlaying with Metal Powders (I) (플라즈마분체 오버레이법에 의한 알루미늄합금 표면의 경화특성에 관한 연구(I) -후막 표면 합금화층의 형성조건과 그 조직-)

  • ;中田一博;;;松田福久
    • Journal of Welding and Joining
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    • v.12 no.4
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    • pp.85-101
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    • 1994
  • Effect of Cr, Cu and Ni metal powders addition on the alloyed layer of aluminum alloy (AC2B) has been investigated with the plasma transferred arc (PTA) overlaying process. The overlaying conditions were 125-200A in plasma arc current, 150mm/min in process speed and 5-20g/min in powder feeding rate. Main results obtained are summarized as follows: 1) It was made clear that formation of thick surface alloyed layer on aluminum alloy is possible by PTA overlaying process. 2) The range of optimum alloying conditions were much wider in case of Cu and Ni powder additions than the case of Cr powder addition judging from the surface appearance and the bead macrostructure. 3) Alloyed layer with Cu showed almost the homogeneous microstructure through the whole layer by eutectic reaction. alloyed layers with Cr and Ni showed needle-like and agglomerated microstructures, the structure of which has compound layer in upper zone of bead by peritectic and eutectic-peritectic reactions, respectively. 4) Microconstituents of the alloyed layer were analyzed as A1+CrA $l_{7}$ eutectics, C $r_{2}$al sub 11/, CrA $l_{4}$, C $r_{4}$A $l_{9}$ and C $r_{5}$A $l_{*}$ 8/ for Cr addition, Al+CuA $l_{2}$(.theta.) eutectics and .theta. for Cu addition, and Al+NiA $l_{3}$ eutectics. NiA $l_{3}$, N $i_{2}$A $l_{3}$ and NiAl for Ni addition. 5) Concerning defect of the alloyed layer, many blow holes were seen in Cr and Ni additions although there was lesser in Cu addition. Residual gas contents in blow hole for Cu and Ni alloyed layer were confirmed as mainly $H_{2}$ and a littie of $N_{2}$ Cracking was observed in compound zone of the alloyed layer in case of Cr and Ni addition but not in Cu alloyed layer.r.r.

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Photoluminescence and Thermal Characteristics of SrAl2O4:Eu+2, Dy+3 Phosphors Synthesized with Various Aluminum Compounds (SrAl2O4:Eu+2, Dy+3 장잔광 형광체 합성에 있어서 알루미늄 화합물에 따른 열적거동 및 발광특성 변화)

  • Lee, Young-Ki;Lee, You-Kee
    • Korean Journal of Materials Research
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    • v.17 no.11
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    • pp.612-617
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    • 2007
  • Both photoluminescence and thermal characteristics for $SrAl_2O_4:Eu^{+2},\;Dy^{+3}$ phosphors synthesized with various aluminum compounds (${\alpha}-Al_2O_3$, ${\gamma}-Al_2O_3$, amorphous-$Al_2O_3$ and $Al(OH)_3)$ were investigated in this study. The formation temperature of the host $SrAl_2O_4$ crystal is changed by these various aluminum compounds, as a result of the different thermal decomposition temperature of $SrCO_3$ phase. Among these compounds, the amorphous-$Al_2O_3$ phase shows the lowest formation temperature of the host $SrAl_2O_4$ crystal. The PL emission and excitation spectra of $SrAl_2O_4:Eu^{+2},\;Dy^{+3}$ phosphor are not affected by these aluminum compounds. After the removal of the Xenon lamp excitation (360 nm), however, the excellent longphosphorescent property of the phosphor is obtained by the amorphous-$Al_2O_3$ phase, although the decay time for all phosphors decrease exponentially.

Formation of Anodized GaN Nanopores on InGaN/GaN Multi-quantum Well Structures (InGan/GaN 다중양자우물구조 위에 제작되어진 산화된 GaN 나노구멍)

  • Choi, Jae-Ho;Kim, Keun-Joo;Jung, Mi;Woo, Deok-Ha
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.11a
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    • pp.315-316
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    • 2006
  • We fabricated GaN nanopores m the etching process of anodic oxidation of aluminum. The aluminum was deposited by using E-beam evaporator on p-type GaN. After the aluminum was anodized GaN structure was exposed to the electric field with the oxidat species. The fabricated nanopore structure provides the enhanced intensity of light emission at the wavelengths 470 nm. We investigated the structure of the GaN nanopores from FE-SEM and EDS measurements.

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A Study on the Removal of Minor Elements from Aluminum Hydroxide with Organic Acids (유기산(有機酸)을 이용(利用)한 Aluminum Hydroxide의 미량원소(微量元素) 제거연구(除去硏究))

  • Lee, Hwa-Young;Cho, Sung-Baek
    • Resources Recycling
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    • v.17 no.5
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    • pp.44-51
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    • 2008
  • The removal of minor elements such as Na, Ca and Fe has been performed from domestic aluminum hydroxide of 99.7% purity with organic acids. Oxalic and citric acid were used as the leaching agent, respectively and aluminum hydroxides of different particle size were also employed for the purification with organic acid leaching. Fine grinding of aluminum hydroxide has been tested using ball mills and leaching characteristics of each element have also been examined in terms of leaching parameters such as temperature, acid concentration, and solid density. As a result, it was found that oxalic acid showed higher leaching efficiency than citric acid in the concentration range of 0.1 to 1.0 mole/l and leaching amount of each element was also increased with the acid concentration and reaction temperature. It was observed that about 45% of Na was leached out during ball milling process which implied that the majority of Na contained in aluminum hydroxide was water soluble compound.

A Study on the Improvement of Fatigue Strength in Particulate Reinforced Metal Matrix Composites at Elevated Temperatures (입자강화 금속기 복합재료의 고온 피로강도 향상에 관한 연구)

  • Sin, Hyeong-Seop
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.5 s.176
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    • pp.1146-1154
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    • 2000
  • Fatigue strength of NiAl and Ni$_3$Al particulate reinforced aluminum alloy composites fabricated by the diecasting method was examined at room and elevated temperatures. The results were compared wit h that of SiC particulate reinforced one. The particulate reinforced composites showed some improvement in the static and fatigue strength at elevated temperatures when compared with that of Al alloy. The composites reinforced by intermetallic compound particles showed good fatigue strengths at elevated temperatures especially $Ni_3AI_{p}/Al$ alloy composite showed good fatigue limit up to high temperature of 30$0^{\circ}C$. Adopting intermetallic compound particle as a reinforcement phase, it will be possible to develop MMC representing better fatigue property at elevated temperature.

Studies on Negative Thermal Expansion in $SrA1_2(BO_3)_2O$ Compound ($SrA1_2(BO_3)_2O$ 화합물에 있어서 열적 수축성 연구)

  • 장기석;이영건;오원균;한범수;더글라스케슬러
    • Korean Journal of Crystallography
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    • v.14 no.1
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    • pp.7-12
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    • 2003
  • The compound SrA1₂(BO₃)₂O is a good host lattice for negative thermal expansion. We have measured thermal expansion over the limited temperature range by X-ray diffraction and ceramic dilatometry. In the aluminum borate compound, a thermal contraction is observed with a coefficient -1.64×10/sup -4/ Å/℃ on the c axis in the temperature range 23∼215℃ and with a maximum change -1.75㎛ in length of a ceramic bar of 20㎜ in the temperature range 110∼170℃, respectively.

The Effect of the Heat Treatment Conditions on the Strength and Microstructure in the Bonded Interface in Dissimilar Metal and Aluminum Alloy (AL합금과 이종금속의 접합계면에서의 미세조직과 접합강도에 미치는 열처리조건의 영향)

  • Kim, Ick-Soo;Choi, Byung-Young;Kang, Chang-Yong
    • Journal of the Korean Society for Heat Treatment
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    • v.16 no.1
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    • pp.2-9
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    • 2003
  • The aluminum alloy which is light and has excellent thermal conductivity and iron base alloy that is remarkable heat-resistece and wear resistence properties were bonded together. The bond was created between a stationary and a rotating member by using the frictional heat generated between them while subjected to high normal forces on the interface of Al alloy and iron base alloy. The microstructure of the bonded interface of friction welding and the strength in the bonded interface formed under various bonding conditions were examined through TEM, SEM with EDX and triple bending test. In interface of bonding materials formed after various heat treatment, bonding strength was substantially different, resulting from formation of intermetallic compound or softening during annealing.

Effect of Al on Structural and Magnetic Characteristics of CoCrFeNiMnAlx High Entropy Alloys

  • Majid Tavoosi;Ali Ghasemi;Gholam Reza Gordani;Mohammad Reza Loghman Estarki
    • Korean Journal of Materials Research
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    • v.33 no.3
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    • pp.95-100
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    • 2023
  • This research examines the effect of adding aluminum on the structural, phasic, and magnetic properties of CoCrFe NiMnAlx high-entropy alloys. To this aim, the arc-melt process was used under an argon atmosphere for preparing cast samples. The phasic, structural, and magnetic properties of the samples were characterized by x-ray diffraction (XRD), scanning electron microscopy (SEM), and vibrational magnetometry (VSM) analyses. Based on the results, the addition of aluminum to the compound caused changes in the crystalline structure, from FCC solid solution in the CoCrFeNiMn sample to CoCrFeNiMnAl BBC solid solution. It was associated with changes in the magnetic property of CoCrFeNiMnAlx high-entropy alloys, from paramagnetic to ferromagnetic. The maximum saturation magnetization for the CoCrFeNiMnAl casting sample was estimated to be around 79 emu/g. Despite the phase stability of the FCC solid solution with temperature, the solid solution phase formed in the CrCrFeNiMnAl high-entropy compound was not stable, and changed into FCC solid solution with temperature elevation, causing a reduction in saturation magnetization to about 7 emu/g.

Effect of Water Content on the Transport of Gemini Surfactant and Hydrophobic Organic Compounds (수분함량이 쌍둥이형 계면활성제 및 소수성 유기오염물질의 거동에 미치는 영향에 관한 연구)

  • Park, In-Sun;Park, Jae-Woo;Cho, Jong-Soo;Hwang, In-Seong
    • Journal of the Korean GEO-environmental Society
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    • v.4 no.2
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    • pp.39-46
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    • 2003
  • An immobilization zone can be constructed by modifying soils in the vadose zone with surfactants, which can be used to promote retardation of organic contaminants in the subsurface. Column experiments were conducted to investigate the behavior of surfactants and organic contaminants in unsaturated and saturated conditions with different water contents (25%, 50%, 75%, 100%). Transport and sorption of surfactant (dialkylated disulfonated diphenyl oxide) in the columns containing aluminum oxide was similar under the conditions at different water contents. However, transport of a model organic compound (naphthalene) was retarded as the water content decreased by enhanced partitioning of the compound into the surfactants that were sorbed on the aluminum oxide. This suggests that the immobilization method could well be applied to vadose zone as well as to saturated zone.

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