• Title/Summary/Keyword: degree of impregnation

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The Impregnation of Thermoplastic Resin into a Unidirectional Fiber Bundle (열가소성 수지 복합재료에서의 수지 함침)

  • Kim, Tae-Uk;Jeon, Ui-Jin;Lee, U-Il
    • 한국기계연구소 소보
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    • s.18
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    • pp.163-168
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    • 1988
  • Impregnation of molten thermoplastic resin into continuous unidirectional fiber bundles was investigated. The degree of impregnation is defined as the ratio between the number of impregnated fibers and the total number of fibers of a bundle. The degree of impregnation was modeled as a function of time, impregnation pressure, temperature and tow size assuming the radial inward flow through the fiber bundle is governed by the Darcy's law. The permeability was assumed to be constant. Experiments were performed to evaluate the validity of the medel. Today's T300 graphite fiber bundles and Polyetheretherketone(PEEK) resin was used. A fiber bundle and resin powder were put into a mold and pressure and temperature were applied. After a predetermined time, the sample was taken out and microphotographs of the cross-section were taken. From the microphotographs, the number of impregnated fibers was counted and then the degree of impregnation was determined. Experiments were also performed for different tow sizes. Good agreements were found between the model and the experiments rendering a confidence in the model.

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Densification Characteristics of Softwood Veneers Treated by Resin Impregnation (침엽수단판의 수지함침처리에 의한 압밀화 특성)

  • 서진석
    • Journal of the Korea Furniture Society
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    • v.14 no.2
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    • pp.21-29
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    • 2003
  • This study was carried out to investigate characteristics of plywood overlaid with softwood veneers densified by resin impregnation and compression. The resin impregnability of Korean pine veneer under atmospheric pressure soaking was greater than that of larch, and impregnability of melamine resin was slightly greater than phenolic resin. It was suggested that resin impregnation ratio was affected by density and thickness of veneer. The largest melamine resin impregnation ratio of 50.7% was obtained with 1.26mm thick Korean pine veneer, and the lowest phenolic resin impregnation ratio of 11.7% with 3.41mm thick larch veneer. Therefore, it was suggested that the vacuum-pres sure-soak treatment is required at thick larch veneer. In densifying resin-impregnated veneers, densification ratio from 13.4 to 31.2% was obtained by high pressure from 15.6 to $20.8kgf/cm^2$. Impregnation of melamine resin also showed relatively greater at densification than that of phenolic resin. So it showed the degree of densification of about 20% or greater. It was seemed that adhesive bonding strength of plywood(base panel) which was directly pressed and overlaid with resin-impregnated veneer was affected by resin tackiness after resin impregnation followed by semi-drying. In laboratory scale, melamine resin impregnation was more favorable for the development of adhesive bonding strength owing to moisture control.

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Fabrication and Characterization Evaluation of Prepreg with Unidirectional Glass Fibers for Use of Automobile Bumper Beams (자동차 범퍼빔용 일방향 유리섬유 프리프레그의 제조 및 특성평가)

  • Kim, Hyoung-Seok;Kim, Jin-Woo;Seo, Jin;Lee, Dong-Gi;Sim, Jae-Ki
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.5
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    • pp.806-811
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    • 2013
  • In this study, to prevent the nonhomogeneity of fiber orientation during the molding of GFRP composites, GFRP prepreg was fabricated using roving fiber and polypropylene resin. Analyses on the degree of impregnation, tensile strength, and microstructure were conducted on the fabricated prepregs. A lower pulling speed, higher resin temperature, and longer die length showed a greater degree of impregnation of the prepreg. The scanning electron microscope (SEM) micrograph showed, a homogeneous fiber orientation. As a result, fundamental techniques for improved productivity were suggested for the manufacturing field.

Development of Multipurpose Seed Paper from Waste Paper ( I ) - Focused on functional chemicals behavior - (폐지를 이용한 기능성 육묘지의 제조(제1보) -기능성 약제의 거동-)

  • Park Soung Bae;Eom Tae Jin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.36 no.4 s.107
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    • pp.41-48
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    • 2004
  • To make a basepaper for multipurposed seed paper, old news print (ONP) and mixed office waste paper (MOW), modified and unmodified with a commercial cellulase, were investigated. Each handsheet was applied with different chemicals such as insecticides, germicides and herbicides. The interactions behaviors of chemicals used with base papers were evaluated by means of the contents of chemicals impregnation and dissolving behaviors in water and soil. The ONP and MOW treated with the cellulase had higher impregnation and dissolving capacities in both water and soil than untreated ONP and MOW. However, the modified ONP showed lower impregnation and dissolving capacities compared to the modified MOW. The content of impregnation of chemicals would be affected with the degree of microfibrils produced by the modification treatment. Otherwise, dissolving capacities of chemicals depend on the affinity of the residual lignin in the paper.

A study on the drawing device and curing mold in CFRP rectangular pipe pultrusion process using a closed impregnation method (밀폐형 함침법을 이용한 CFRP 사각 파이프 인발성형에서 인발장치 및 경화금형에 관한 연구)

  • Kang, Byung-Soo;Yoo, Hyeong-Min
    • Design & Manufacturing
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    • v.16 no.2
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    • pp.60-65
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    • 2022
  • In the pultrusion process for the CFRP (Carbon fiber reinforced plastic) rectangular pipe, the drawing device is eseential which can continuously produces products and draws the carbon fiber tow. In addition, since the degree of cure changes depending on the temperature and the temperature ditribution of the curing mold changes depending on the pultrusion speed, the temperature distribution of the curing mold under certain conditions must be studied before processing. In this study, in the pultrusion process using a closed impregnation method, which has several advantages compared to the general pultrusion process using a open bath impregnation method, the drawing force required to pull the carbon fiber tows and the temperature distribution of the curing mold was analyzed to design the drawing device and the curing mold efficiently.

Manufacture of Continuous Glass Fiber Reinforced Polylactic Acid (PLA) Composite and Its Properties (연속 유리섬유 강화 폴리유산 복합재료의 제조 및 물성)

  • Roh, Jeong U;Lee, Woo Il
    • Composites Research
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    • v.26 no.4
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    • pp.230-234
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    • 2013
  • The continuous glass fiber reinforced poly-lactic acid (PLA) composite was manufactured by direct melt impregnation. The mechanical and thermal properties of continuous glass fiber reinforced PLA composite were observed. Measured properties were compared with the reference values of neat PLA and the injection molded glass fiber/ PLA composite. The continuous glass fiber reinforced PLA composite having a fiber volume fraction of 27.7% shows enhanced tensile strength of 331.1 MPa, flexural strength of 528.6 MPa, and flexural modulus of 24.0 GPa. The enhanced heat deflection temperature (HDT) and the increased cystallinity were also observed. The degree of impregnation as a function of pulling speed was also assessed. The degree of impregnation at the pulling speed of 5 m/min was over 90% in this research.

Fabrication of isotropic bulk graphite using artificial graphite scrap

  • Lee, Sang-Min;Kang, Dong-Su;Kim, Woo-Seok;Roh, Jea-Seung
    • Carbon letters
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    • v.15 no.2
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    • pp.142-145
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    • 2014
  • Isotropic synthetic graphite scrap and phenolic resin were mixed, and the mixed powder was formed at 300 MPa to produce a green body. New bulk graphite was produced by carbonizing the green body at $700^{\circ}C$, and the bulk graphite thus produced was impregnated with resin and re-carbonized at $700^{\circ}C$. The bulk density of the bulk graphite was $1.29g/cm^3$, and the porosity of the open pores was 29.8%. After one impregnation, the density increased to $1.44g/cm^3$ while the porosity decreased to 25.2%. Differences in the pore distribution before and after impregnation were easily confirmed by observing the microstructure. In addition, by using an X-ray diffractometer, the degrees-of-alignment (Da) were obtained for one side perpendicular to the direction of compression molding of the bulk graphite (the "top-face"), and one side parallel to the direction of compression molding (the "side-face"). The anisotropy ratio calculated from the Da-values obtained was 1.13, which indicates comparatively good isotropy.

Improvement of Fast-Growing Wood Species Characteristics by MEG and Nano SiO2 Impregnation

  • DIRNA, Fitria Cita;RAHAYU, Istie;ZAINI, Lukmanul Hakim;DARMAWAN, Wayan;PRIHATINI, Esti
    • Journal of the Korean Wood Science and Technology
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    • v.48 no.1
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    • pp.41-49
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    • 2020
  • Jabon (Anthocephalus cadamba) is a fast-growing wood species that is widely utilized for light construction and other purposes in Indonesia. The objectives of the current study were to determine the effects of monoethylene glycol (MEG) and SiO2 nanoparticles (nano SiO2) impregnation treatment on the dimensional stability and density of jabon wood and to identify the characteristics of impregnated jabon wood. Wood samples were immersed in water (as untreated), MEG, 0.5% MEGSiO2, then impregnated by applying 0.5 bar of vacuum for 60 min, and then applying 2.5 bar of pressure for 120 min. The results showed that impregnation with MEG and Nano SiO2 had a significant effect on the dimensional stability of jabon wood. Polymers can fill cell walls in wood indicated by increasing weight percentgain, antiswelling efficiency, bulking effect, and density, then decreasing in water uptake value. Jabon wood morphology by using SEM showed that MEGSiO2 polymers can cover part of the pitsin the wood vessel wall of jabon. This finding was reinforced by EDX results showing that the silicon content was increased due to the addition of SiO2 nano. The XRD diffraction pattern indicated that MEGSiO2 treatment increased the degree of crystallinity in wood samples. Overall, treatment with 0.5% MEGSiO2 led to the most improvement in the dimensional stability of 5-year-old jabon wood in this study.

Manufacturing of GFRP Sheet Using Plain Weaving Method (평직직조방법을 적용한 GFRP Sheet 제조에 관한 연구)

  • Kim, in Woo;Kim, Hyoung Seok;Lee, Jung Hoon;Lee, Dong Gi
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.38 no.8
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    • pp.849-855
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    • 2014
  • The GFRP composite is used for hot press flow molding of automotive components, and the different flow rates of fiber and plastic are likely to induce fiber orientation and inhomogeneity in the material. However, very limited systematic research studies are available on composite materials with superior flow homogeneity and optimized fiber orientation. The inhomogeneity and fiber orientation issues of GFRP composites have still not been resolved through research. The plain weaving method applied to the GFRP prepreg can improve its recyclability, inhomogeneity, fiber flow, structural stability, fiber deformation, surface smoothness, degree of impregnation, and other mechanical properties. The need for more detailed and thorough studies is evidenced.

A STUDY ON THE RESIN IMPREGNATION AND SHEAR BOND STRENGTH BY VARIOUS DENTIN CONDITIONERS (수종 상아질 표면처리제에 의한 레진 침투 및 전단결합강도에 관한 연구)

  • Lee, Kwang-Won;Lee, Myung-Jong
    • Restorative Dentistry and Endodontics
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    • v.15 no.1
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    • pp.201-216
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    • 1990
  • A variety of surface pre-treatments have been advocated to prepare the dentin prior to placement of a bonding agent. The purpose of this study was to evaluate the effect of various dentin conditioners upon the degree of resin impregnation to the dentinal tubules and the shear bond strength of a new dentinal bonding agent (Scotchbond 2) used in conjunction with a visible light cured composite (Silux). The healthy eighty human molars extracted due to periodontal or orthodontic reasons were used and randomly divided into five groups. All the grinded dentin surfaces were conditioned with 3% $H_2O_2$, Cavity Cleanser (Columbus/Bayer), Dentin Conditioner (GC Inter. Corp.), Scotchprep (3M Co.) according to the manufacturer's directions. The specimens were then demineralized in 10% HCl for 20 sec. and 24 hrs. in order to observe the resin tags in Hitachi X-450 scanning electron microscope at 25KV. Also, shear strengths were obtained using an Instron Testing Machine with a cross head speed of 1 mm/min. The following results were obtained ; 1. In group treating with Dentin Conditioner and Scotchprep, the resin strings were formed on most of the surfaces and penetrated more than $50{\mu}m$ into the tubules. 2. The inner surface of resin treated with Cavity Cleanser, indicating the resin strings formed partly and penetrated about in depth of $30{\mu}m$. 3. In control and experimental group treated with 3% $H_2O_2$, the resin tags were not formed, if any, penetrated shortly. 4. Shear bond strengths in groups treating with Dentin Conditioner and Scotchprep were statistically significant increase than with 3% $H_2O_2$. (P<0.01). 5. The Scotchprep treatment group was significantly higher in shear strength than groups treated with no conditioning and Cavity Cleanser.(P<0.01) 6. Shear bond strengths evaluated were gradually increase in proportion to the tag length of resin impregnation.

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