• 한국자기학회지
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• 제9권3호
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• pp.127-130
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• 1999

사각형구조를 갖는 Ru 단층에서 살창상수와 자성과의 관계를 총 에너지 총 퍼텐셜 보강 평면 파동(FLAPW) 에너지띠 방법에 의해 연구하였다. 반강자성상태를 고려하기 위해 2개의 원자를 포함하는 사각형에서 살창상수가 7.30a.u.보다 큰 경우는 강자성이었고 그 보다 작은 경우에는 상자성이었다. 반강자성상태도 고려하였으나 총 에너지 계산결과 그 가능성은 없었다. 총 에너지 최소값은 살창상수가 6.53a.u.인 경우로 이 때의 자기적 상태는 상자성이었다. Ag의 살창상수값 근처인 7.72a.u.에서 자기모멘트는 2.49$\mu$B로 계산되었다. 살창상수가 7.86a.u.인 경우에 자기모멘트가 거의 포화되었으며 그 때의 자기모멘트는 2.57$\mu$B이었다.

• Journal of Magnetics
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• 제13권2호
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• pp.61-64
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• 2008

We studied the effect of the variation of the lattice constant on the electrical properties of $SrRuO_3$ thin films. In order to obtain films with different volumes, we varied the substrate temperature and oxygen pressure during the growth of the films on $SrTiO_3$ (001) substrates. The films were grown using a pulsed laser deposition method. The X-ray diffraction patterns of the grown films at low temperature and low oxygen pressure indicated the elongation of the c-axis lattice constant compared to that of the films grown at a higher temperature and higher oxygen pressure. The in-plane strain states are maintained for all of the films, implying the expansion of the unit-cell volume by the oxygen vacancies. The variation of the electrical resistance reflects the temperature dependence of the resistivity of the metal, with a ferromagnetic transition temperature inferred form the cusp of the curve being observed in the range from 110 K to 150 K. As the c-axis lattice constant decreases, the transition temperature linearly increases.

• 한국전기전자재료학회논문지
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• 제18권9호
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• pp.846-850
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• 2005

[ $SrTiO_3$ ]:Al, Pr red phosphors for FED were synthesized by solid state reaction method. The dependence of their luminescent properties on Sr and Al concentration was investigated. The $SrTiO_3$: Al, Pr phosphors showed the characteristic X-ray diffraction patterns of the perovskite structure. Photoluminescence intensity and lattice constant in $SrTiO_3$: Al, Pr phosphors changed in quite a similar manner with Sr concentration. Photoluminescence intensity increased with increasing lattice constant, and the decrease of photoluminescence intensity and lattice constant occurred in the vicinity of 1 mol Sr concentration.

• Applied Microscopy
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• 제41권1호
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• pp.75-79
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• 2011

For quantitative analysis of nano-crystal structure, we reported the accuracy improvement method of lattice parameters measured from electron diffraction. For calculation of Au lattice parameters used as a standard crystal structure, it was considered two different acquisition methods (detector and enegy-filter) and three different calculation methods (conventional, least-square and regression fit). As a result, the measurement reliability could be enhanced by using CCD camera which gives higher performance, while energy-filtering did not affect the improvement the camera constant accuracy. Also, the accuracy of lattice parameters could be improved up to $10^{-4}$ order by regression fitting with correction formula. Finally, it is expected that the combination of regression fitting and intensity extraction from energy-filtered precession electron diffraction gives a solution of quantitative structure analysis for unknown nano-crystals.

• 한국산학기술학회논문지
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• 제18권10호
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• pp.97-101
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• 2017

X-선 회절기(X-ray diffractometer)는 시편에서 회절되는 회절빔을 이용하여 재료의 상 (phase), 집합조직 (texture), 격자상수 (lattice constant), 잔류응력 (residual stress) 등 다양한 재료물성을 분석하는 데 광범위하게 사용되는 장치이다. X-선을 이용한 정량적인 분석은 회절빔의 피크 위치를 바탕으로 수행되는 데, 장시간 X-선 회절기를 사용하게 되면 필연적으로 장치 부품에 미세 변형이 발생하게 되고, 이러한 기계적인 오차가 발생하면 정량적인 분석의 정확도가 떨어지게 된다. 본 연구에서는 미국 표준기술연구소 (National Institute of Standards and Technology, NIST)에서 제공된 잔류응력이 없는 Si 파우더를 이용하여 $2{\theta}$를 기준으로 약 30~90도 사이 구간에 대해 X-선 회절 실험을 수행하였고, NIST에서 제공된 회절빔의 피크 위치와의 비교를 통하여 X-선 회절기의 계통오차를 파악하였으며, 이러한 오차 교정이 진격자상수 (true lattice constant) 측정 등 정량적인 분석에 미치는 영향을 확인하기 위하여 잔류응력이 존재하는 180 nm 두께의 텅스텐 박막에 대한 X-선 회절 분석을 수행하였다.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1095-1096
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• 2006

When $Y_2O_3$ was added to Ti-excess $BaTiO_3$ ((Ba+Y)/Ti =1), the area occupied by $Y^{3+}$ ion was confirmed by its microstructure development, electrical conductivity behavior and lattice constant. Grain growth inhibition was observed when the content of donor dopant exceeded a critical value ($x{\approx}.0.01$) in $BaTiO_3+x(0.5Y_2O_3+TiO_2)$ system. A donor-doped behavior was observed at various Y contents ($0.2\sim3.0$ mol% Y) when $Y_2O_3$ was added to $TiO_2$-excess $BaTiO_3$. As Y content was increased, (002) and (200) peaks shifted to higher angles and the lattice constant (a and c axis) decreased gradually.

• 한국전기전자재료학회논문지
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• 제24권7호
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• pp.599-604
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• 2011

A highly strained nanostructure comprising crystallographically aligned HgTe nanoinclusions and a surrounding PbTe matrix has been synthesized using a precipitation process of supersaturated HgTe-PbTe alloys. From the early precipitation stage, HgTe nanoinclusions take disk shape, which is transformed from initial HgTe nuclei, although there is no lattice constant difference of the two end components at standard state. As a primary reason for the morphological transformation of the initial spherical HgTe nuclei to HgTe nanodisks, the induced lattice mismatch is suggested. On the condition that the HgTe nanodisks maintain perfect coherent nature with PbTe matrix, the stress-free lattice constant of constrained HgTe nanodisks has been calculated based on the defined concept of the strain-induced tetragonality, the linear elasticity and the actual measurement in HRTEM images.

• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2009년도 9th International Meeting on Information Display
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• pp.942-944
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• 2009

Blue phase shows several different reflection colors from the randomly oriented domains and crystal direction. Also there are variations in the size of domains. The domain size is dependent on the temperature gradient. With smaller cooling rate of temperature, the domain size was increased compared with rapid cooling. With injection of light of specific wavelength, we find that the diffraction patterns were occurred around the light spot in the cell of blue phase. It was supposed to be from the matching of the phase retardation and domain size. However, actually the diffraction pattern is reflecting the lattice structure in double twist of the blue phase. The lattice constant from the radius of diffraction patterns shows very similar one from the reflection spectrum, which indicates the internal lattice constant in double twist of the blues phase.

• 대한화학회지
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• 제15권4호
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• pp.165-169
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• 1971

A general method of calculating the frequency shift due to lattice defects is developed for a one dimensional lattice with an arbitrary number of lattice points. The method is based on the Fourier transform of the equation of motion. It is shown that the frequency spectrum is determined by the roots of 5${\times}$5 secular equation, the coefficients of which depend on defects in the mass and the force constant as well as the number of the lattice points. For the limiting case of infinite lattice, the dimension of the secular equation reduces to three and the result agrees with that of Montroll and Potts.

• Progress in Superconductivity
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• 제7권1호
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• pp.64-68
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• 2005

We fabricated Ni-based alloy substrates for YBCO coated conductor using powder metallurgy. Tungsten and copper were selected as alloy elements due to their mutual solubility to the base element of nickel. The alloying elements were mixed with nickel using ball milling and dried in air. The powder mixtures were packed in a rubber mold, cold isostatic pressed 200 MPa and made into rods. The compacted rods were sintered at $1150^{\circ}C$ for 6 hours for densification. It was confirmed by neutron diffraction experiment that W and Cu atoms made complete solid solution with Ni. Lattice constant of nickel alloy increased by $0.004{\AA}$ for 1at. $\%$ W in Ni-W alloy, $0.0006{\AA}$ for 1 at. $\%$ Cu in Ni-W-Cu alloy.