• Title/Summary/Keyword: microstructure

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Influence of negative bias voltage on the microstructure of Cr-Si-N films deposited by a hybrid system of AIP plus MS (Negative bias voltage effect에 따른 Cr-Si-N 박막의 미세구조에 대한 연구)

  • Sin, Jeong-Ho;Kim, Gwang-Ho
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2009.05a
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    • pp.130-131
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    • 2009
  • AIP(arc ion plating)방법과 마그네슘 스퍼터링(DC reactive magnetron sputtering) 방법을 결합시킨 하이브리드 코팅 시스템으로 Cr-Si-N 코팅막을 합성하였다. 고분해능 TEM 및 SEM 분석들로부터 negative bias voltage에 따른 미세구조의 영향을 나타내었다. negative bias voltage의 증가에 따라 columnar microstructure가 amorphous microstructure로 변화하였다. bias voltage effect에 의해 Cr-Si-N 코팅막내 입자의 크기가 미세해지고 나노 복합체를 잘 형성하였다.

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Microstructure and High Temperature Strength of Rapidly Solidified Al-8wt%Fe Alloy (급속응고된 Al-8wt%Fe 합금의 미세조직 및 고온강도)

  • 최병준
    • Journal of Powder Materials
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    • v.5 no.3
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    • pp.192-198
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    • 1998
  • Microstructure and mechanical properties were examined on rapidly solidified Al-8wt%Fe alloy. High temperature strength test was also undertaken, and it is shown that the refinement in microstructure resulting from extremely rapid cooling rates gives rise to improved high temperature strength, but the elongation to fracture of this material decreases with increasing temperature, particularly in the temperature range up to 30$0^{\circ}C$. Specimens heat-treated for 100 hrs were analyzed with TEM micrographs to understand the thermal stability of this material.

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The Effect of Solvent Treatment on the Microstructure and Surface Morphology of PET POY (폴리에스테르 부분배향사의 용매처리에 따른 내부구조 및 표면형태의 변화)

  • 신혜원;유효선
    • Journal of the Korean Society of Clothing and Textiles
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    • v.20 no.3
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    • pp.467-480
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    • 1996
  • Interactions between PET POY and solvents were estimated by the changes in microstructure and surface morphology. Changes in microstructure and surface morphology by the solvent treatments were: an increase in crystallite size, a decrease in interplanar spacing, a change in degree of orientation of crystalline region, a change in surface characteristics.

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Microstructure, mineralogy and physical properties: techniques and application to the Pusan Clay

  • Locat, Jacques;Tanaka, Hiroyuki
    • Proceedings of the Korean Geotechical Society Conference
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    • 1999.11b
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    • pp.15-31
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    • 1999
  • The Pusan Clay is analyzed hereafter from a point of view of mineralogy and microstructure. Results indicate that the Pusan Clay is basically illitic in nature and that the soil microstructure reveals some characteristics which could be responsible for its brittle behavior as observed from sample disturbance. The overall analysis would tend to consider that the Pusan Clay profile analyzed here shows mechanical properties similar to well structured soils or so-called cemented soils.

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Computer Simulation of Microstructure Evolution during Hot Forging of Waspaloy (미세조직 변화를 고려한 열간 단조 공정에서의 유한요소해석)

  • Kang, G.P.;Lee, K.H.;Lee, S.U.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.10a
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    • pp.53-56
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    • 2007
  • Computer simulation of microstructure evolution during hot forging process is of great interest in recent years. Recrystallization model and grain growth model which use a phenomenological approach were summarized. For the waspaloy, upsetting process and cogging process were simulated using $DEFORM^{TM}$ and the change in grain size were investigated in each deformation procedure.

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Development of P/M Aluminum Alloy with Fine Microstructure

  • Tokuoka, Terukazu;Kaji, Toshihiko;Nishioka, Takao
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.712-713
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    • 2006
  • We successfully developed Al-Si-Transition Metal (TM) -Rare Earth (RE) Powder Metallurgy (P/M) alloy with fine microstructure, which has high strength at high temperature. This material was compacted rapidly solidified powder and directly consolidated by hot extruding or forging. Before consolidating, rapid heating was performed on powder compaction in order to keep the fine microstructure in powder state. We have also investigated the processing conditions of this new alloy by computing simulations and experiments.

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Characteristics and microstructure of MCFC electrode (용융탄산염형 연료전지 전극의 미세구조와 특성)

  • 김귀열;엄승욱
    • Electrical & Electronic Materials
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    • v.8 no.5
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    • pp.544-550
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    • 1995
  • In this paper, the anode for molten carbonate fuel cell have been prepared by doctor blade method and microstructure, pore distribution, sintering test of the electrode were investigated. Component analysis were done by Scanning Electron Micrograph, porosimeter and sintering test apparatus. As a result, median pore size was 11.mu.m order at the major specimen and porosity was about 70%. And thickness loss of the electrode was 1.5% at Ni-10Co anode after sintering test.

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Texture and Rolling Characteristics of AZ31 Magnesium Alloy (AZ31 마그네슘의 집합조직변화와 압연특성)

  • Akramov, S.;Kim, In-Soo
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.05a
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    • pp.480-481
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    • 2008
  • The aim of this work is to compare the microstructure, the texture, of an AZ31 Mg alloy processed via cold rolling process. Initial AZ31 Mg alloy sheet samples with strong {0002} texture were cut along the angles of 12.5 and 25 degrees to normal direction (ND). These specimens were rolled in room temperature condition. The microstructure was characterized by optical microscopy and the texture was measured by X-ray diffraction.

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Influence of negative bias voltage on the microstructure of CrN films deposited by arc ion plating (Negative bias voltage effect에 따른 CrN 박막의 미세구조에 대한 연구)

  • Sin, Jeong-Ho;Kim, Kwang-Ho
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2009.10a
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    • pp.159-160
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    • 2009
  • AIP(arc ion plating)방법으로 CrN 코팅막을 합성하였다. 고분해능 SEM과 AFM 분석들로부터 negative bias voltage에 따른 미세구조의 영향을 나타내었다. negative bias voltage의 증가에 따라 columnar microstructure가 amorphous microstructure로 변화하였다. bias voltage effect에 의해 CrN 코팅막내 입자의 크기가 미세해지고 나노 복합체를 잘 형성하였다.

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Atomic Scale Investigation of TRIP Steels (변태 유기 소성강(TRIP steel)의 미세구조와 원자 단위 분석)

  • Lim, N.S.;Kang, J.S.;Kim, S.I.;Park, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.10a
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    • pp.273-276
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    • 2008
  • In this study, microstructure and distribution of alloy elements were investigated in thermo-mechanically processed C-Mn-Si transformation induced plasticity (TRIP) steels. The microstructures of TRIP steels were investigated by using advanced analysis techniques, such as three dimensional atom probe tomography (3D-APT). At first, the microstructure was observed by using TEM. TEM results revealed that microstructure of C-Mn-Si TRIP steel was composed of ferrite, bainte, and retained austenite. 3D-APT was used to characterize atomic-scale partitioning of added elements at the phase interface. In the retained austenite phase, Ti and B were enriched with C. However, there was no fluctuation of Mn and Si concentration across the interface. Through these analysis techniques, the advanced characteristics of constituent microstructure in C-Mn-Si TRIP steels were identified.

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