• Title/Summary/Keyword: optical microscopic analysis

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Quantitative Analysis of Mineral Composition in Porland Cement Clinker by X-ray Diffraction (포틀랜드 시멘트 클린커 광물조성의 X선구절에 의한 정량분석)

  • Chang, Se-Kyung;Rhee, Jhun;Han, Ki-Sung
    • Journal of the Korean Ceramic Society
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    • v.23 no.2
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    • pp.64-70
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    • 1986
  • In this investigation x-ray diffraction method was mainly studied for quantitative analysis of clinker mineral composition. And also optical microscopic observation and Bogue calculation method were applied to compare with the x-ray diffraction method. In the procedure of x-ray diffraction analysis graphite monochromator automatic divergence slit and spinner for sample holder were used for minimizing the error due to the operation of the equipment. Especially the separation of overlapped peaks were proceeded by micro-processor automatically. The results of x-ray diffraction method for synthesized clinker were consistent with the Bogue value and the results of optical microscopic observation. However the results of quantitative analysis of mineral composition or commercial clinker containing solid solution of minor component were different from the Bogue value. On the other hand they agreed reasonably well with results of the optical mic-roscopic observation.

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Heterocyclic Nonlinear Optical Chromophores Composed of Phenothiazine or Carbazole Donor and 2-Cyanomethylene-3-cyano-4,5,5-trimethyl-2,5-dihydrofuran Acceptor

  • Cho, Min-Ju;Kim, Ja-Youn;Kim, Jae-Hong;Lee, Seung-Hwan;Dalton, Larry R.;Choi, Dong-Hoon
    • Bulletin of the Korean Chemical Society
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    • v.26 no.1
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    • pp.77-84
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    • 2005
  • We prepared the new nonlinear optical chromophores that show fairly high microscopic nonlinearity through intramolecular charge transfer. Phenothiazine and carbazole units played an important role to contribute high electron donability and connect the resonance pathway via conjugative effect in the cyclized ring beside the aromatic ring. Theoretical calculation, electrochemical analysis, and absorption spectroscopic study gave us useful information about the energy states and microscopic nonlinearities of two serial chromophores. We compared the microscopic nonlinearities of four chromophores with the conjugation length and electron donability in the push-pull type NLO chromophores. The effect of gradient donability and lengthening the conjugation were investigated on the electronic state and microscopic nonlinearity.

A comparison of Modified One Layer Vasovasostomy with Optical Loupe and Microscope (Optical Loupe와 현미경을 이용한 단층정관정관문합술의 비교)

  • Kim, Jong-Gu;Cho, In-Rae;Park, Seok-San;Choi, Hee-Seok
    • Clinical and Experimental Reproductive Medicine
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    • v.27 no.1
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    • pp.99-105
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    • 2000
  • Objective: The objective of this study was to compare results of the macroscopic one-layer vasovasostomy with those of microscopic one-layer vasovasostomy and to analyze the change of semen parameters according to the interval of vasal obstruction. Method and Materials: Between March 1987 and December 1997, we performed 121 vasovasostomies using modified one-layer technique with loupe magnification (macroscopic vasovasostomy) or microscope. Among the 68 could be followed post-operatively, 37 patients were treated by macroscopic technique with loupe, and 31 patients by microscopic technique. We compared rates of anatomical patency (sperm count above than $10{\times}10^{6}$/ml) and pregnancy of macroscopic vasovasotomy with those of microscopic vasovasostomy. Patency and pregnancy rates according to vasal obstructive interval were also examined. Results: The patency rates of macroscopic and microscopic technique were 86.5% and 87.1%, and pregnancy rates of macroscopic and microscopic technique were 64.9% and 67.7%. There was no statistical significance between these two methods (p>0.05). The pregnancy rates and sperm motility were decreased if more than 10 years had elapsed following vasectomy (p<0.05). Conclusion: We found little difference in success rates resulting from macroscopic and microscopic vasovasostomy and the former had the advantage of reduced cost and a lower operator skill level. In post-operative semen analysis, the sperm motility was the most probable factor associated with vasal obstructive interval.

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Study on the Optical Analysis Equipment Control System for Electronic Parts Inspection (전자 부품 검사용 광학분석 장비 제어시스템에 대한 연구)

  • Lee, Jun Ha
    • Journal of the Semiconductor & Display Technology
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    • v.14 no.4
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    • pp.67-71
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    • 2015
  • Product of technology developed in this study is an external interface for controlling the equipment of pendant key remote control system circuit board, and it is used in the electronic component test equipment system. Main control system module is in the role as a device for controlling the various control devices that make up the integrated system for microscopic examination at the request of the host computer engineers to control the inspection equipment. The pentane-key interface module to its role as a device for controlling the various control devices that make up the integrated system for microscopic examination at the request of the host computer for the engineer to control the inspection equipment. Development of the control system can be expected in the configuration of a system for efficient and accurate inspection of high-precision parts.

Simulation of Rough Surface of CIGS (CuInGaSe) Solar Cell by RCWA (Rigorous Coupled Wave Analysis) Considering the Incoherency of Light

  • Kim, Sung Chul
    • Journal of the Optical Society of Korea
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    • v.18 no.2
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    • pp.180-183
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    • 2014
  • The surface of semiconductor solar cells, such as a-Si or CIGS (CuInGaSe) solar cells is not flat but textured in the microscopic domain. With textured surfaces, the optical reflectivity of a solar cell is different from that of flat surfaces in the wavelength region. In this paper, the effects of a textured surface on a CIGS solar cell are presented by RCWA (Rigorous Coupled Wave Analysis) method. The effect of incoherent light is also considered by RCWA with a Fourier analysis while conventional optical simulation uses the input light on the solar cell as coherent light. Using experimental results, the author showed that the RCWA method with a Fourier analysis is a proper method to simulate the optical properties of CIGS solar cells.

Surface orientational distributions of chiral chitosan-polymer (카이랄 키토산 고분자의 표면 방향 분포 연구)

  • N. Y. Ha;S. H. Han;H. J. Chang;J. S. Hwang;D. W. Jeon;Jung, Chi-Sup;Park, Byoungchoo;J W. Wu
    • Proceedings of the Optical Society of Korea Conference
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    • 2003.07a
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    • pp.168-169
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    • 2003
  • We have determined the orientational distribution functions (OBFs) at both air and substrate isotropic interfaces of a chiral chitosan bio-polymer film by the measurements of surface second-harmonic generation (SHG). It was shown that the simultaneous SHG analysis of both interfaces, based on the macroscopic and microscopic relations, provides all the informations on the nonlinear optical (NLO) activity. (omitted)

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Heat treatment characteristics of medium carbon steel by CW Nd:YAG Laser (CW Nd:YAG 레이저를 이용한 중탄소강의 열처리특성)

  • Shin H.J.;Yoo Y.T.;Ahn D.G.;Im K.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.438-443
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    • 2005
  • Laser surface hardening is an effective technique used to improve the tribological properties and also to increase the service life of automobile components such as camshafts, crankshatfs, lorry brake drums and gears. High power CO2 lasers and Nd:YAG lasers are employed for localized hardening of materials and hence are of potential application in the automobile industries. The heat is conducted rapidly into the bulk of the specimen causing self-quenching to occur and the formation of martensitic structure. In this investigation, the microstructure features occurring in Nd:YAG laser hardening SM45C steel are discussed with the use of optical microscopic and scanning electron microscopic analysis. Moreover, This paper describes the optimism of the processing parameters for maximum hardened depth of SM45C steel specimens of 3mm thickness by using CW Nd:YAG laser. Travel speed was varied from 0.6m/min to 1.0m/min. The maximum hardness and case depth fo SM45C steel are 780Hv and 0.4mm by laser hardening.

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Surface Heat treatment of Die material by means of CW Nd:YAG Laser (CW Nd:YAG레이저를 이용한 금형 재료의 표면열처리)

  • Yoo Young-Tae;Shin Ho-Jun;Jang Woo-Yang
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.13 no.5
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    • pp.67-74
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    • 2004
  • Laser heat treatment is an effective technique used to improve the tribological properties and also to increase the service life of automobile components such as camshafts, crankshatfs, lorry brake drums and gears. High power $CO_2$ lasers and Nd:YAG lasers are employed for localized hardening of materials and hence are of potential application in the automobile industries. The heat is conducted rapidly into the bulk of the specimen causing self-quenching action to occur and the formation of matrensitic structure. In this investigation, the microstructrual features occurring in Nd:YAG laser hardening SM45C and $STD_11$ steel are discussed with the use of optical microscopic and scanning electron microscopic analysis. Moreover, This paper describes the optimisation of the processing parameters for maximum hardened depth of SM45C and $STD_11$ steel specimens of 10mm thickness by using CW:YAG laser.

Metallic pattern Heat treatment by means of CW Nd:YAG Laser (CW Nd:YAG 레이저를 이용한 금형열처리)

  • Shin, Ho-Jun;Yoo, Young-Tae;Oh, Yong-Seak;Ro, Kyoung-Bo
    • Proceedings of the KSME Conference
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    • 2003.11a
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    • pp.1898-1904
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    • 2003
  • Laser heat treatment is an effective technique used to improve the tribological properties and also to increase the service life of automobile components such as camshafts, crankshatfs, lorry brake drums and gears. High power $CO_{2}$ lasers and Nd:YAG lasers are employed for localized hardening of materials and hence are of potential application in the automobile industries. The heat is conducted rapidly into the bulk of the specimen causing self-quenching to occur and the formation of matrensitic structure. In this investigation, the microstructrual features occurring in Nd:YAG laser hardening SM45C and $STD_{11}$ steel are discussed with the use of optical microscopic and scanning electron microscopic analysis. Moreover, This paper describes the optimisation of the processing parameters for maximum hardened depth of SM45C and $STD_{11}$ steel specimens of 10mm thickness by using CW Nd:YAG laser.

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