• Title/Summary/Keyword: powder mixture

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EffEct of vacuum annealing on an oxidation of milled WC-Co powder (분쇄된 초경합금 분말의 산화에 미치는 진공열처리 효과)

  • 김소나
    • Journal of Powder Materials
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    • v.3 no.2
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    • pp.91-96
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    • 1996
  • The effect of vacuum annealing on the oxidation behavior of milled WC-15%Co powder mixture has been studied. A cobalt component in the milled powder mixture was oxidized preferentially above 175$^{\circ}C$ in air. The specimens showed a steady increase in weight at 175$^{\circ}C$ but did constant weight followed by rapid increase in specimen weight at the beginning above 20$0^{\circ}C$. Oxidation of the milled powder mixture was significantly suppressed by vacuum annealing at 30$0^{\circ}C$ for 10 h. Suppression of oxidation by vacuum annealing and different oxidation behaviors of the milled powder mixture between 175$^{\circ}C$ and 20$0^{\circ}C$, were attributed to removal of strain energy stored in the cobalt powder during vacuum annealing or oxidation treatment above 20$0^{\circ}C$. The role of stored strain energy on oxidation of milled WC-15%Co powder mixture was proved by X-ray diffraction method and differential thermal analysis.

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Physical Properties of Reinforced Soil-Mixture Powder (보강혼합토분의 물리적 특성)

  • 이상호;차현주;김철영;장병욱
    • Proceedings of the Korean Society of Agricultural Engineers Conference
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    • 1999.10c
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    • pp.336-340
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    • 1999
  • This study was performed to evaluate the physical properties of reinforced soil-mixture powder. Soil was used to be powder that passed by the No. 200 mech and the reinforcement as calcium carbonate, quicklime and portland cement used for this study to improve soil. We resulted from fineness , setting time, and compressive strength test of reinforced soil-mixture powder. We've got the two conclusions . The first , in case that we were used reinforced soil-mixture powder included some portland cement, the higher the mixture rates of the reinforcement , the wider the difference theoretical data with experimental data. The second, the setting time of reinforced soil-mixture powder is faster than soil powder itself and the reinforcement for promoting strength was proved that calcium carbonate was proper than others if we compared it with other reinforcment.

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Spark-Plasma Sintering of Mechanically-alloyed NiAl Powder and Ball-milled (Ni+Al) Powder Mixture (기계적합금화 NiAl 분말과 볼밀혼합된 (Ni+Al) 분말의 방전플라즈마소결)

  • 장영일;김지순;안인섭;김영도;권영순
    • Journal of Powder Materials
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    • v.7 no.3
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    • pp.161-167
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    • 2000
  • Mechanically-alloyed NiAl powder and ball-milled (Ni+Al) powder mixture were sintered by spark-plasma sintering(SPS) process. Mechanical alloying was performed in a horizontal attritor for 20 h with rotation speed of 600 rpm. (Ni+Al) powder mixtures were prepared by ball milling for 1 and 10 h with 120 rpm. Both powders were sintered at $1150^{\circ}C$ for 5 min under $10^{-3}$ torr vacuum with 50 MPa die pressure in a SPS facility. Sintered densities of 97% and 99% were obtained from mechanically-alloyed NiAl powder and (Ni+Al) powder mixture, respectively. The sintered compact of (Ni+Al) powder mixture showed large grain size by a very rapid grain growth, while the grain size of mechanically-alloyed NiAl powder compact after sintering was extremely fine(80 nm). The difference in densification behavior of both powders were discussed.

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Effect of Cobalt Oxide on Carbothermal Reduction of Spray Dried Titanium-Cobalt-Oxygen Based Oxide Powder (분무건조법에 의해 제조된 Ti-Co-O계 산화물 분말의 환원/침탄반응에 미치는 코발트 산화물의 영향)

  • Lee, Gil-Geun;Kim, Chan-Young
    • Journal of Powder Materials
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    • v.12 no.5 s.52
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    • pp.336-344
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    • 2005
  • In the present study, the focus is on the effect of cobalt oxide powder in the carbothermal reduction of the titanium-cobalt-oxygen based oxide powder by solid carbon for the optimizing synthesis process of ultra fine TiC/Co composite powder. The titanium-cobalt-oxygen based oxide powder was prepared by the combination of the spray drying and desalting processes using the titanium dioxide powder and cobalt nitrate as the raw materials. The titanium-cobalt-oxygen based oxide powder was mixed with carbon black, and then this mixture was carbothermally reduced under flowing argon atmosphere. Changes in the phase structure and thermal gravity of the mixture during carbothermal reduction were analysed using XRD and TGA. Titanium-cobalt-oxygen based oxide powder desalted at $600^{\circ}C$ had a mixture of $TiO_2\;and\;Co_{3}O_4$. And the one desalted at $800^{\circ}C$ had a mixture of $TiO_2\;and\;CoTiO_3$. In the case of the former powder, the reduction of cobalt oxide powder in the titanium-cobalt-oxygen based oxide powder occurred at lower temperature than the latter one. However, the carbothermal reduction of titanium dioxide powder in the titanium-cobalt-oxygen based oxide powder with a mixture of $TiO_2\;and\;Co_{3}O_4$ occurred at higher temperature than the one with a mixture of $TiO_2\;and\;CoTiO_3$. And also, the former powder showed a lower TiC formation ability than the latter one.

Physical properties of Reinforced soil Mixture powder (보강혼합토분의 물리적 특성)

  • 이상호
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.42 no.5
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    • pp.125-132
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    • 2000
  • This study was performed to evaluate the physical properties of reinforced soil mixture powder. Soil sample was prepared by passing into the standard sieve of No. 200 and reinforcement materials were calcium carbonate, quicklime and portland cement. Fineness, setting time, and compressive strength test for reinforced soil mixture powder were performed and analyzed to investigate their physical properties. The main results were summarized as follow. The compressive strength of soil mixture powder itself and most reinforced was reinforced according to increasing in the mixture rate of reinforcement and the rate of increase was remarkably higher in the cement reinforced soil moisture powder. It was appeared that the early compressive strength is considering higher in the cement reinforced soil moisture powder with 2% of moisture rate of accelerator.

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Properties of Compacts and Pellets Made Using Bimodal- Sized $UO_2$ Powder

  • Kim, Keon-Sik;Song, Kun-Woo;Kang, Ki-Won;Kim, Jong-Hun;Kim, Young-Min
    • Nuclear Engineering and Technology
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    • v.31 no.6
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    • pp.608-617
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    • 1999
  • The powder mixture which has a bimodal size distribution, with a large mode corresponding to AUC-UO$_2$ powder and a small one corresponding to ADU-UO$_2$ powder, was prepared, pressed into compacts, and sintered at 1680t for 4 hours in hydrogen gas. The compact density of the powder mixture increases with increasing ADU-UO$_2$content within a content of 20 wt %, since small ADU-UO$_2$ particles can fill interstices between large AUC-UO$_2$particles. The UO$_2$ pellet made using the powder mixture has a lower open porosity than that made using AUC-UO$_2$ powder alone. The mechanism for the formation of a flake-like pore is proposed, and the decrease in open porosity may be ascribed to the decrease in the number of flake-like pores.

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An Experimental Study on the Setting Time and Compressive strength of Mortar using Ferronickel Slag Powder (페로니켈슬래그 미분말을 사용한 모르타르의 응결시간 및 압축강도특성에 관한 실험적 연구)

  • Kim, Young-Uk;Kim, Do-Bin;Choi, Se-Jin
    • Journal of the Korea Institute of Building Construction
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    • v.18 no.6
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    • pp.551-558
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    • 2018
  • This study evaluate the fluidity and hardening properties of mortar by replacement ratio of ferronickel slag powder to estimate the applicability of ferronickel slag powder for cement replacement materials. Ferronickel slag powder was replaced by 0, 5, 10, 15 and 20% of the cement weight. In addition, blast furnace slag powder and fly ash were also used for comparing with the mixtures using ferronickel slag powder. As the test results, the micro-hydration heat of the mixture containing the ferronickel slag powder was lower than that of the mixtures containing the same amount of blast furnace slag powder and fly ash. The flow of the sample with ferronickel slag powder was relatively higher than the other mixtures. In all ages, the compressive strength of the mixture with ferronickel slag powder and fly ash was similar to that of the mix containing only fly ash. In case of drying shrinkage, the mixture containing ferronickel slag powder exhibited lower drying shrinkage than the mixture using blast furnace slag powder, and similar to the mixture containing fly ash.

Densification of Metal Injection Molding Parts Made of Ball Milled W-20%Cu Powders (볼밀링한 W-20wt%Cu 분말로 제조된 금속사출성형 부품의 조밀화)

  • 김순욱;류성수;문인형
    • Journal of Powder Materials
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    • v.7 no.4
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    • pp.228-236
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    • 2000
  • An investigation was carried out on the possibility whether the ball-milling process of low energy could successfully improve the packing density and flowability for MIM application in W-20wt%Cu system. In this study, W-20wt%Cu powder mixture was prepared by ball-milling. W powder was not fractured by low mechanical impact energy used in the present work during the critical ball-milling time, but the ductile Cu powder was easily deformed to the 3 dimensional equiaxed shape, having the particle size similar to that of W powder. The ball-milled mixture of W-20wt%Cu powder had the more homogeneous distribution of each component and the higher amount of powder loading for molding than the simple mixture of W-Cu powder with an irregular shape and a different size. Accordingly, the MIM W(1.75)-20wt%Cu powder compacts were able to be sintered to the relative density of 99% by sintering at $1400^{\circ}C$ for one hour.

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Effects of Mineral Powder on Performance of Warm Reclaimed Asphalt Mixture

  • Liu, Yao;Wang, Xiao-Yong
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2018.05a
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    • pp.216-217
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    • 2018
  • The three kinds of tests are used to further study the effect of the amount of mineral powder in this mixture design. Firstly, comparing the relationship of the content of mineral powder and asphalt bitumen membrane thickness at different asphalt content, through film thickness to determine the range of gradation and asphalt content in laboratory tests, Grade A and Grade D, asphalt content 2.6%, 3.4% and 3.8% are set for the benchmark, then fatigue properties of the test are carried out in the established range, the result show that asphalt film thickness decreases with the addition of mineral powder. The result also show that fatigue properties of asphalt rubber mixture will reduced, when mineral powder added in, especially when the asphalt content is high.

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