• Title/Summary/Keyword: pressure curing

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Solidification/Stabilization of Dyeing Sludge Treated by Fenton Reagent Using Blast Furnace Slag and Fly Ash

  • Lee, Sookoo;Kim, Sebum
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.453-458
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    • 2001
  • This study was performed to reuse the dyeing wastewater sludge treated by Fenton process through the solidification/stabilization technique. To solidify the dyeing sludge the industrial by-products such as blast furnace slag, fly ash and waste sand with cement were used. The laboratory scale and pilot scale test were conducted at room temperature to make construction brick which has high compressive strength and low leaching of heavy metals. The experimental results showed that blast furnace slag and fly ash could be used instead of cement and the products satisfied the regulation of Korean Standards. The blast furnace slag increased the compressive strength and the optimum ratio of slag/dyeing sludge on dry basis was found 0.4. The solidifying agent of SB series could increase rapidly the compressive strength and the optimum ratio of solidifying agent/sludge on dry basis was 0.26 at which the strength was two times compared with non-added condition. The portion of waste and industrial by-products in matrix was over 80%. From the pilot test the optimum pressure in molding was 100kg/$\textrm{cm}^2$ at which the compressive strength was over 100kg/$\textrm{cm}^2$. And the strength increased continuously to 160kg/$\textrm{cm}^2$ until 120 days curing time due to pozzolanic reaction. When SB-20 as a solidifying agent was used, the unconfined compressive strength of dyeing sludge could be obtained 110kg/$\textrm{cm}^2$ which satisfied the regulation of cement brick in Korea Standard(KS).

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A Study on the Preparation of Durable Softening Water Repellents by Blends of Fatty Carbamide/Wax/Acrylic Copolymer(III);Water Repelling Treatment of Nylon Fabrics (지방산 카르바미드/왁스/아크릴 공중합체의 블렌드에 의한 내구유연발수제의 제조에 관한 연구(III);나일론 직물에의 발수처리)

  • Kim, Seung-Jin;Im, Wan-Bin;Ahn, Chong-Il;Park, Hong-Soo
    • Journal of the Korean Applied Science and Technology
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    • v.11 no.2
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    • pp.69-74
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    • 1994
  • Durable softening water repellents for nylon fiber were synthesized, using two compounds: quaternized octadecyl methacrylate-2-diethylaminoethyl methacrylate copolymer as a mother resin of water repellent and quaternized fatty carbamide for improving softness and hydrostatic pressure, of which syntheses were studied in the previous papers. They were blended with waxes and emulsifiers in a variety of ratios and synthesized into water repellent PADWC, and it was nylon taffeta treated with and without textile finishing resin. The synthesized water repellents can be used either or without resin. The optimum curing temperature was 150 to 160$^{\circ}C$ and the optimum concentration was 3 to 5wt%. In the independent and conjunct treatment, the water repellency of nylon taffeta samples have no remarkable changes between initial value and that after three times washing, so these prove that the synthesized compounds are durable water repellent. The water repellency of PADWC-3 and -4 were around 90. Also, comparison of crease recovery and tear strength after repelling treatment showed that the synthesized water repellents have a very high softening effect.

Influence of Milk Co-precipitates on the Quality of Restructured Buffalo Meat Blocks

  • Kumar, Sunil;Sharma, B.D.;Biswas, A.K.
    • Asian-Australasian Journal of Animal Sciences
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    • v.17 no.4
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    • pp.564-568
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    • 2004
  • Restructuring had made it possible to utilize lower value cuts and meat trimmings from spent animals by providing convenience in product preparation besides enhancing tenderness, palatability and value. Milk co-precipitates (MCP) have been reported to improve the nutritional and functional properties of certain meat products. This study was undertaken to evaluate the influence of incorporation of milk co-precipitates at four different levels viz. 0, 10, 15 and 20% on the quality of restructured buffalo meat blocks. Low-calcium milk co-precipitates were prepared from skim milk by heat and salt coagulation of milk proteins. Meat chunks were mixed with the curing ingredients and chilled water in a Hobart mixer for 5 minutes, followed by addition of milk co-precipitates along with condiments and spice mix and again mixed for 5 minutes. Treated chunks were stuffed in aluminium moulds and cooked in steam without pressure for 1.5 h. After cooking, treated meat blocks were compared for different physico-chemical and sensory attributes. Meat blocks incorporated with 10% MCP were significantly better (p<0.05) than those incorporated with 0, 15 and 20% MCP in cooking yield, percent shrinkage and moisture retention. Sensory scores were also marginally higher for meat blocks incorporated with 10% MCP than product incorporated with 15 and 20% MCP, besides being significantly higher than control. On the basis of above results 10% MCP was considered optimum for the preparation of restructured buffalo meat blocks. Instrumental texture profile analysis revealed that meat blocks incorporated with 10% MCP were significantly better (p<0.05) in hardness/ firmness than control although, no significant (p>0.05) differences were observed in cohesiveness, springiness, gumminess and chewiness of both type of samples.

Synthesis and Characterization of Photosensitive Polyimides Containing Alicyclic Structure (지방족고리 구조를 함유하는 감광성 폴리이미드 수지의 합성 및 특성 평가)

  • 심종천;최성묵;심현보;권수한;이미혜
    • Polymer(Korea)
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    • v.28 no.6
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    • pp.494-501
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    • 2004
  • A new alkali developable photosensitive poly(amic acid) (PAA-0) with transmittance at 400 nm was synthesized from cyclobutane-1,2,3,4-tetracarboxylic dianhydride, 2-(methacryloyloxy)ethyl-3,5-diamino-benzoate and 1,3-bis(3-aminopropyl)-1,1,3,3-tetramethyl disiloxane in N-methyl-2-pyrrolidinone. Photosensitivity of the PAA-0 was investigated at 365-400 nm in the presence of a photoinitiator using a high pressure mercury lamp. The photo-cured poly(amic acid) was insoluble toward aqueous 2.38 wt% tetramethylammonium hydroxide solution. Negative pattern of the PAA-0 with 25 ${\mu}{\textrm}{m}$ resolution was obtained by developing with 2.38 wt% tetramethylammonium hydroxide solution after exposure of 600 mJ/$\textrm{cm}^2$ in the presence of 2,2-dimethoxy-2-phenyl-acetophenone as a photoinitiator. The patterned poly(amic acid) was converted to polyimide by thermal curing at 25$0^{\circ}C$ for 50 min, which showed chemical resistance against photoresist stripper as well as good transmittance at 400 nm.

A study on the dependance of crucible dimension on AlN single crystal growth (AlN 단결정 성장에 관한 도가니 형태의 의존성에 관한 연구)

  • Yin, Gyong-Phil;Kang, Seung-Min
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.25 no.1
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    • pp.1-5
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    • 2015
  • For the special usage, the effort of developing AlN single crystals has been very hot in the world. The AlN-base UV LEDs are used on the field of sterilization, purification, curing and analyzing, which can advance human's living and medical processes etc.. AlN single crystals were grown by the PVT (Physical vapor transport) method. On the growing process, carbon crucibles with three different types such as normal size, taller than normal and wider than normal were used for comparison. The processing temperature was in the range of $1900{\sim}2100^{\circ}C$ and ambient pressure was 200~1 Torr. When the taller crucible was used, the sublimation mass was greater than normal dimension one but the best condition of growth changes widely. However the wider one gave much sublimation mass and growing condition was more stable than normal dimension. On limited growing furnace system, the changes of crucible dimension of PVT method provide the change of best condition for growth rate, as-grown crystal quality and growth condition stability.

Magnetorheological Elastomer Based on Reactive Blend of Maleic Anhydride Grafted Chloroprene Rubber and Epoxidized Natural Rubber (말레무수물로 개질된 클로로프렌 고무와 에폭시화 천연고무의 반응 블렌드에 기초한 자기유변 탄성체)

  • Choi, Jinyoung;Chung, Kyungho
    • Elastomers and Composites
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    • v.49 no.4
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    • pp.267-274
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    • 2014
  • Self vulcanizable blend system for magnetorheological elastomer (MRE) has been studied by dispersing magneto responsible particle (MRP) on elastomeric matrix. Chloroprene rubber was modified with maleic anhydride (MAH) using heat and pressure which is called dynamic maleation process. The optimum graft ratio of MAH was found at 10 phr contents and reaction temperature of $100^{\circ}C$. This could be confirmed by FT-IR analysis. Epoxided natural rubber (ENR) was blended with modified CR-g-MAH for self vulcanization. The optimum amounts of ENR was 30 wt% in terms of scorch time and curing rate. MRE was manufactured by electromagnetic equipment and orientation of MRE was confirmed by SEM. Finally, it was found that the tensile strength of anisotropic-MRE was higher than that of isotropic-MRE and the hardness was reverse.

Development of Shading Tape for Manufacturing of Touch Panel Display with High Screen-to-Body Ratio (기기 면적 대비 높은 화면 비율을 갖는 터치 패널 디스플레이 제조를 위한 차광 테이프의 개발)

  • Kim, Ki-Chul
    • Journal of Convergence for Information Technology
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    • v.7 no.4
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    • pp.75-81
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    • 2017
  • The design trend of information technology is quickly changed with the times. The design trend of information display is a bezel-less display, recently. The bezel-less display or edge-less display is a new trend of mobile phone display. In this study, the shading tape was manufactured for assembling process of touch panel display with the high screen-to-body ratio so-called bezel-less display. The shading tape was fabricated on PET film with the UV curable acrylic pressure sensitive adhesive(PSA) by roll-to-roll process. The UV curable PSA was synthesized with the eco-friendly toluene-less manufacturing method. The adhesive power of manufactured shading tape was investigated by motorized tensile testing machine. The thixotropic, maintaining property of cutting shape, was characterized by field emission scanning electron microscope. As results, the shading tape exhibits high adhesive power and good thixotropic performance suitable for assembly process of touch panel display. The functional shading tape will be expected to improve productivity of assembly process of touch panel display.

Effect of Fiber Addition for Improving the Properties of Lightweight Foamed Concrete (경량 기포콘크리트의 성능향상에 대한 섬유혼입의 영향)

  • Lee, Kyung-Ho;Yang, Keun-Hyeok
    • Journal of the Korea Institute of Building Construction
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    • v.15 no.4
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    • pp.383-389
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    • 2015
  • The objective of this study is to develop mixture proportioning approach of crack controlled lightweight foamed concrete without using high-pressure steam curing processes, as an alternative to autoclaved lightweight concrete blocks (class 0.6 specified in KS). To control thermal cracks owing to hydration heat of cementitious materials, 30% ground granulated blast-furnace slag (GGBS) was used as a partial replacement of ordinary portland cement (OPC). Furthermore, polyvinyl alcohol (PVA) and polyamid (PA) fibers were added to improve the crack resistance of foamed concrete. The use of 30% GGBS reduced the peak value of hydration production rate measured from isothermal tests by 28% and the peak temperature of foamed concrete measured from semi-adiabatic hydration tests by 9%. Considering the compressive strength development, internal void structure, and flexural strength of the lightweight foamed concrete, the optimum addition amount of PVA or PA fibers could be recommended to be $0.6kg/m^3$, although PA fiber slightly preferred to PVA fiber in enhancing the flexural strength of foamed concrete.

Memory Effect of $In_2O_3$ Quantum Dots and Graphene in $SiO_2$ thin Film

  • Lee, Dong Uk;Sim, Seong Min;So, Joon Sub;Kim, Eun Kyu
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.240.2-240.2
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    • 2013
  • The device scale of flash memory was confronted with quantum mechanical limitation. The next generation memory device will be required a break-through for the device scaling problem. Especially, graphene is one of important materials to overcome scaling and operation problem for the memory device, because ofthe high carrier mobility, the mechanicalflexibility, the one atomic layer thick and versatile chemistry. We demonstrate the hybrid memory consisted with the metal-oxide quantum dots and the mono-layered graphene which was transferred to $SiO_2$ (5 nm)/Si substrate. The 5-nm thick secondary $SiO_2$ layer was deposited on the mono-layered graphene by using ultra-high vacuum sputtering system which base pressure is about $1{\times}10^{-10}$ Torr. The $In_2O_3$ quantum dots were distributed on the secondary $SiO_2$2 layer after chemical reaction between deposited In layer and polyamic acid layer through soft baking at $125^{\circ}C$ for 30 min and curing process at $400^{\circ}C$ for 1 hr by using the furnace in $N_2$ ambient. The memory devices with the $In_2O_3$ quantum dots on graphene monolayer between $SiO_2$ thin films have demonstrated and evaluated for the application of next generation nonvolatile memory device. We will discuss the electrical properties to understating memory effect related with quantum mechanical transport between the $In_2O_3$ quantum dots and the Fermi level of graphene layer.

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Heavy-impact sound insulation performance according to the changes of dry flooring structure in wall structure

  • Cho, Jongwoo;Lee, Hyun-Soo;Park, Moonseo;Lim, Hohwan;Kim, Jagon
    • International conference on construction engineering and project management
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    • 2017.10a
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    • pp.89-98
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    • 2017
  • The floor heating method generally uses a wet construction method including the installation of resilient material, lightweight foam concrete, heating piping, and finishing mortar. Such a wet construction method not only delays other internal finishing processes during curing period for two mortar pouring process, but also has a disadvantage that it is difficult to replace the floor heating layer when it deteriorated because it is integrated with the frame. Dry floor heating construction method can be a good alternative in that it can solve these defects. Conversely, when it applied to the wall structure that is vulnerable to the interlayer noise compared with the column-beam structure, the question about the heavy-impact sound(HIS) insulation performance is raised. Therefore, conventional dry floor heating method is hard to apply to the wall structure apartments. Therefore, for the purpose to improve the applicability of dry floor heating method in wall structure apartments, this study investigated the change of floor impact sound, especially HIS insulation performance which is one of the required performance for the floor structure. This study tried to examine whether the change of heavy-impact sound pressure level(SPL) shows a tendency at the significant level according to the shape and mass of the floor structure. Through filed experiments on wall structure apartment, this study confirmed that the form of the raised floor shows better HIS insulation performance than the fully-supported form. In addition, it was also confirmed that the HIS insulation performance increases with the mass on the upper part. Moreover, this study found the fact that a mass of about 30 kg/m2 or more should be placed on the upper structure to reduce the heavy-impact SPL according to the bang machine measuring method. Although this study has a limit due to insufficient experiment samples, if the accuracy of this study is increased, it will contribute to the diffusion of dry floor heating by setting the HIS insulation performance target and designing the dry floor heating structure that meets the target.

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