• Title/Summary/Keyword: scanning electron microphotographs

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Effect of surface treatment of graphene nanoplatelets for improvement of thermal and electrical properties of epoxy composites

  • Kim, Minjae;Kim, Yeongseon;Baeck, Sung Hyeon;Shim, Sang Eun
    • Carbon letters
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    • v.16 no.1
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    • pp.34-40
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    • 2015
  • In this study, in order to improve the thermal and electrical properties of epoxy/graphene nanoplatelets (GNPs), surface modifications of GNPs are conducted using silane coupling agents. Three silane coupling agents, i.e. 2-(3,4-epoxycyclohexyl)-ethyltrimethoxysilane (ETMOS), 3-glycidoxypropyltriethoxysilane (GPTS), and 3-glycidoxypropyltrimethoxysilane (GPTMS), were used. Among theses, GPTMS exhibits the best modification performance for fabricating GNP-incorporated epoxy composites. The effect of the silanization is evaluated using transmission electron microscopy (TEM), scanning electron microscopy, thermogravimetric analysis, and energy dispersive X-ray spectroscopy. The electrical and thermal conductivities are characterized. The epoxy/silanized GNPs exhibits higher thermal and electrical properties than the epoxy/raw GNPs due to the improved dispersion state of the GNPs in the epoxy matrix. The TEM microphotographs and Turbiscan data demonstrate that the silane molecules grafted onto the GNP surface improve the GNP dispersion in the epoxy.

Rhipicephalus sanguineus (Latreille 1806); A new Record of Male Tick Identified with Scanning Electron Microscopy in Korea (Rhipicephalus sanguineus에 대한 최초(最初)의 국내보고(國內報告)와 수컷에 대한 주사전자현미경적관찰(走査電子顯微鏡的觀察))

  • Kang, Yung bai
    • Korean Journal of Veterinary Research
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    • v.24 no.2
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    • pp.201-211
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    • 1984
  • Rhipicephilus sanguineus (Latreille 1806) the brown dog tick, is one of the most widely distributed ixodid ticks in the world, however, there was no report for the discovery of the species in Korea. Specimens unfed or partly fed were collected from the dogs rearing in the livestock farms and the pastures near the farms located in Kyunggi-Do, Chungchong-Namdo, Cholla-Pukdo and Cheju-Do, in summer seasons during 1981 to 1984. The specimens were examined at the Institute of Veterinary Research in Anyang and were identified as R. sanguineus. The morphological characteristics observed by means of the scanning electron microscope were presented with some SEM microphotographs. As. R. sanguineus is firstly discovered to occur in Korea, a total of 20 species of ticks belonging to E: genera, such as, Argas, Amblyomma, Boophilus, Dermacentor, Haemaphysalis, Hyalomma, Ixodes and Rhipicephilus, has now been recorded.

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Scanning Electron Microscopic Observations on the Surface Structure of the Tick, Haemaphysalis longicornis Neumann 1901 (주사전자현미경(走査電子顯微鏡) 영상분석(映像分析)에 의한 haemaphysalis longicornis 의 표면(表面) 미세구조(微細構造))

  • Kang, Yung bai;Jang, Du hwan
    • Korean Journal of Veterinary Research
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    • v.24 no.2
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    • pp.213-226
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    • 1984
  • Scanning electron microscope (Model; SEM ISI-DS-130) was used to observe the fine surface structures of the predominant cattle tick Haemaphysalis longicornis Neumann 1901 (Acarina: Ixodidae) in Korea and some SEM microphotographs were presented in this pictorial monograph. Brief descriptions of the main contents are consisted of followings; L Mean body size is 2.43mm in unfed males and 2. 58mm in unfed females, the eyes are absent. 2. The scutums are inornated but there are some short-setae on the surface of the body. 3. The festoons on the dorso-marginal part of the body are present and segmented with 11 sectors. 4. The cornua is well-developed and the bypostome dentition is usually 5/5 in both sexes but rarely 4/4 also seen. 5. There is no dorsal projection on the anteriointernal margin of the palpal article 2, howevever, there are well developed dorso-internal setae with setal fossa on it. 6. The joints of the legs (Coxatrochanter and trochanter coxa, etc) are well developed.

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IN VITRO STUDY ON THE EFFECTS OF THE FLOURIDE ON THE REMINERALIZATION OF ACID ETCHED ENAMEL (불소가 산부식된 법랑질의 재석회화에 미치는 영향에 관한 연구)

  • Kim, Jin-Han;Lee, Ki-Soo
    • The korean journal of orthodontics
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    • v.26 no.4
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    • pp.389-399
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    • 1996
  • Remineralization of acid-etched enamel across the time has been one of the curiosities in the context of the orthodontic biomechanics(Arends J. et al., IRL Press, 1, 1985), nevertheless, is so far controversial. It was the aim of this study to observe the remineralization patterns of acid-etched enamel across the time and whether the existence of fluoride might carry out any modifications. The intact buccal surfaces of the first bicuspids which was extracted for orthodontic treatment were ground smooth, and etched with a 38w/w% phosphoric acid for 60 seconds, The surface was observed by the scanning electron microscope and surface microhardness was measured after immersion in the fluoride or non-fluoride containing remineralizing solution for 0 hour, 12 hours, 1 day, 3 days, 7 days, 14 days, 28 days, and 42 days. The following results and conclusions were drawn; 1. Surface microhardness increased in both fluoride containing and non-fluoride containing solution group with time lapse. 2. In fluoride containing solution group, the surface microhardness sharply increased at the 12 hours group, on the other hand, surface microhardness increased at 3 days in non-fluoride containing solution group. 3. The difference in microhardness value between two groups manifested gradual decrease. 4. Scanning electron microphotographs disclosed that the fluoride containing solution group generated spiculate sub-stances in the 12 hours group, which was increased in number and size with time lapse. 7 days later, spherical composure was began to be produced, The spiculate substances so much increased in number that the etched enamel surface looked like flat in 42 days. 5. In non fluoride-containing solution group, there was no surface change at 42 days, perceivable in scanning electron microphotographs which could be defined as remineralization though the surface was a little rougher than the incipient etched surface. These results demonstrate that the action of the fluoride is exceedingly pertinent in the remineralization of acid-etched enamel and the remineralization process goes uninterruptedly with time lapse.

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Holocene Paleoenvironmental Changes and Characteristic of Diatom Distribution in Upo Wetland of Korea (우포늪의 홀로세 동안 퇴적환경 변화 및 돌말류 분포 특성)

  • Lee, Hoil;Lee, Sang Deuk;Lee, Jin-Young;Lim, Jaesoo;Kwon, Daeryul;Park, Mirye;Yun, Suk Min
    • Korean Journal of Ecology and Environment
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    • v.53 no.2
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    • pp.109-137
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    • 2020
  • Upo Wetland is the largest riverine wetland in Korea which has been inscribed on the Ramsar List of Wetlands of International Importance in 1998. In this study, sedimentological study was carried out in order to understand the environmental changes in Upo Wetland during the Holocene. The drilling work for recovering the Quaternary sediments was conducted on the inner part (UPW17-01, UPW17-02, and UPW17-03) and the outer part (UPL17-01, UPL17-02) of the Upo Wetland. The recovered sediments are commonly characterized by gravel-dominated deposits in the lower part and silty clay-dominated deposits in the middle to upper parts respectively, which are seemed to be changed from fluvial to palustrine/lacustrine environments around 4,000 cal yr BP. In order to establish the Holocene diatoms distribution from Upo Wetland, we identified 63 diatom taxa. Of these, 14 species were new records for Korea: Gomphonema consector, Gomphonema jadwigiae, Hantzschia abundans, Luticola pseudomurrayi, Luticola spauldingiae, Neidium suboblongum, Ninastrelnikovia gibbosa, Oricymba rhynchocephala, Pinnularia borealis var. lanceolata, Pinnularia latarea, Pinnularia paliobducta, Pinnularia saprophila, Sellaphora laevissima, Stauroneis pseudoschimanskii. All identified diatom species are illustrated by high-quality scanning electron microscopic and light microscopic microphotographs. The ecological habitat for all taxa are presented.

Enhancement of Antioxidant Activities of Blueberry (Vaccinium ashei) by Using High-Pressure Extraction Process (초고압 처리가 블루베리의 항산화 증진에 미치는 영향)

  • Park, Sung Jin;Choi, Young Bum;Ko, Jung Rim;Kim, Young Eon;Lee, Hyeon Yong
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.43 no.3
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    • pp.471-476
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    • 2014
  • We developed a method for improving the antioxidant activities of blueberry (Vaccinium ashei) extracts through an ultra high-pressure extraction process. Blueberries were subjected to water extraction at $60^{\circ}C$ and 300 MPa for 5 min (High Pressure Extraction, HPE5) and 15 min (HPE15). Extraction yields obtained by ultra high-pressure extraction process were 18.48, and 19.89%, respectively. Total polyphenol contents were estimated to be 28.3, and 28.9 mg/g, whereas flavonoid contents were measured as 5.9 and 6.0 mg/g, respectively. Generally, HPE resulted in higher yields than the conventional extraction process. Further, HPE15 showed 53.84% DPPH radical scavenging activity (EDA, %) at $1,000{\mu}g/mL$. Reducing power of HPE15 showed its highest activity of 0.21. In general, antioxidant activities of blueberry increased by HPE. Therefore, HPE of blueberry resulted in higher antioxidant activity than conventional water extraction. These results demonstrate obvious advantages in terms of higher efficiency, shorter extraction time, and lower energy costs.

Exploration of Optimum Retention of Antibacterial Agents in Functional Packaging Paper (항균 포장원지내 항균소재의 최적 정착법 탐색)

  • Kim, Chul-Hwan;Kim, Jae-Ok;Jung, Jun-Ho;Cho, Sung-Hwan
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.34 no.2
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    • pp.298-305
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    • 2005
  • Antimicrobial packaging paper was prepared with a powder-type botanical antimicrobial agent from grapefruit seed extract (BAAG) and zeolite according to TAPPI standard method. The functional fillers containing BAAG fixed to CaCO$_3$ and zeolite were well retained in the fiber network by a retention aid such as cationic polyacrylamide, which was ascertained by the ash contents of paper and the SEM microphotographs. With addition of the functional fillers to paper, tensile strength and burst strength of the paper decreased by interference of the functional fillers with interfiber bonding but bending stiffness and tear strength increased by improved elastic modulus of paper and delayed transfer of tearing energy. Finally, it was confirmed that the antimicrobial packaging paper might be able to be used to make packaging bags and corrugated containers due to the minor deterioration of strength properties.

Chemical Composition of Precipitation in Suwon Area and Its Effect on Crop Development (수원지역(水原地域) 강우(降雨)의 성분조성(成分組成)과 작물(作物)에 미치는 영향(影響))

  • Lee, Jong-Sik;Kim, Bok-Young;Woo, Ki-Dae
    • Korean Journal of Environmental Agriculture
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    • v.13 no.1
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    • pp.31-38
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    • 1994
  • This study was carried out to investigate the possibility of potential injury to crops which were exposed to precipitation. The rainwater were collected from May to September in 1992 and analyzed its chemical composition. The amounts of chlorophyll and cations in plant were measured, and the morphological structure of epidermis was also investigated by SEM. The results are summarized as follows: 1. The pH of precipitation in Suwon was relatively high even with high level of $SO_4^{2-}$ and monthly pH at May, June, July, August, and September were 4.65, 5.47, 5.32, 5.44 and 4.80, respectively. 2. The amount of ions in rainwater was in the order of $NH_4^+$, $Ca^{2+}$, $Mg^{2+}$ and $H^+$ for cations, and $SO_4^{2-}$, $NO_3^-$ and $Cl^-$ for anions. 3. pH of rain in less than 5mm of precipitation was higher than that in greater than 5mm of precipitation. 4. The amount of chlorophyll was higher in the plant exposed to rain than that in plant intercepted rain during the early portion of growing season, but at the later period, the trend was shown to be reversed. 5. When the sesame plants were exposed to rain at harvesting stage, they contained less amount of CaO, MgO and $Na_2O$ than those with the interception of rain. 6. Scanning electron microphotographs revealed the shringkage in glandular trichomes in the epidermis of sesame leaves when they were exposed to rain.

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The Effect of EDTA, Tetracycline-HCl, and Citric Acid on Diseased Root Surfaces; The SEM Study (EDTA, 염산 테트라싸이클린, 구연산 처치가 치근면에 미치는 영향)

  • Ahn, Seong-Hee;Chai, Jung-Kiu;Kim, Chong-Kwan;Cho, Kyoo-Sung
    • Journal of Periodontal and Implant Science
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    • v.29 no.3
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    • pp.561-578
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    • 1999
  • The goal of periodontal therapy is the periodontal regeneration by the removal of microorganisms and their toxic products from the periodontally diseased root surface. To achieve periodontal regeneration, root conditioning as an adjunct to root planing has been done. There are low pH etchants such as citric acid, tetracycline-HCl, and EDTA solution which is a neutral chelating agent. The purpose of present study was to examine the effect of root conditioning by citric acid, tetracycline HCl, and EDTA. Total 35 root specimens(6${\times}$3${\times}$2mm) were prepared from the periodontally diseased teeth, scaled and root planed. The specimens were treated with normal saline for 1 minute, saturated citric acid(pH 1) for 3 minutes, 50mg/ml tetracycline-HCl(pH 2) for 5 minutes, 15% EDTA(pH 7) for 5 minutes using rubbing technique. The specimens were examined under scanning electron microscopy at 1000, and 3000 magnification. On the microphotographs taken at 1000 magnification, the numbers of opened and patent dentinal tubules per unit area(10,640${\mu}m^2$) were counted. And the diameters of opened dentinal tubules per unit are (10,640${\mu}m^2$) were measured. The differences of number and diameter among all groups were statistically analyzed by Kruskal Wallis Test. The results were as follows; 1. In the specimens applied with normal saline(control group), the root surface was finely cracked, and was covered by irregular smear layer. Neither exposed dentinal tubules nor any patent dentinal tubules could be seen. 2. In the specimens applied with saturated citric acid(experimental 1 group), the globular collagen fibers were exposed around the peritubular space, and many dentinal tubules were revealed. 3. In the specimens applied with tetracycline-HCl(experimental 2 group), the process-like collagen fibers were exposed around the peritubular space, and some dentinal tubules were revealed. 4. In the specimens applied with 15% EDTA(experimental 3 group), the root surface was covered by the collagenous fibrillar network, and many dentinal tubules were revealed. 5. The numbers of opened and patent dentinal tubules were significantly more in exp. 1 group and exp. 3 group than in exp. 2 group(P<0.05). But there was no significant difference between exp. 1 group and exp. 3 group. In control group, the number of opened and patent dentinal tubules could not be counted because any dentinal tubules couldn't be seen. 6 . The diameter of opened dentinal tubules was significantly smaller in exp. 1 group and exp. 3 group than in exp. 2 group(P<0.05). But there was no significant difference between exp. 1 group and exp. 3 group. In control group, the diameter of opened dentinal tubules could not be measured because any dentinal tubules couldn't be seen. The results demonstrate that root conditioning with citric acid, tetracycline- HCl, and EDTA is more effective in periodontal healing than only root planing, and 15% EDTA solution can replace low pH etching agents such as citric acid, tetracycline-HCl for root conditioning.

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