• Title/Summary/Keyword: ultrasonic bath

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Determination the optimum extraction method for saponin lancemasides in Codonopsis lanceolata (더덕 사포닌인 lancemasides의 최적 추출 방법 구명)

  • Lee, Min Ju;Nam, Ju Hee;Um, In Eeok;Kang, Chang Keun;Rho, Il Rae
    • Korean Journal of Food Science and Technology
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    • v.51 no.2
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    • pp.103-108
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    • 2019
  • This study was conducted to select the optimal extraction method of codonopsis lanceolata saponin. To investigate the lancemasides content depending on each extraction method, various extractions were performed: reflux (methanol and butanol), hot water, as well as ultrasonic bath (40 kHz; continuous irradiation/interval irradiation) and ultrasonicator (20 kHz) extractions. From the result, the overall lancemasides content were the highest in ultrasonic bath (MeOH; continuous irradiation) extraction, followed by ultrasonic bath (water; continuous irradiation)>ultrasonic bath (MeOH; interval irradiation)>ultrasonicator (MeOH)>hot water>MeOH reflux>BuOH reflux extractions in that order. Sample drying method prior to ultrasonic bath extraction was more effective shade drying than freeze drying. Effective duration and temperature of extraction was 2 hr at $64^{\circ}C$. And ingredient change diverted from aster saponin Hb to lancemasides was identified by extraction condition such as extraction time and temperature.

Effect of Ultrasonic Bath in Preparing Specimens for Transmission Electron Microscopy (전자현미경 시료 제작에 있어 Ultrasonic bath의 유용성에 관한 연구)

  • Lim, Byung-Soo;Choi, Jeung-Mok;Kang, Dae-Young
    • Applied Microscopy
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    • v.28 no.3
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    • pp.315-328
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    • 1998
  • The present study was carried out to investigate the effect of ultrasonic bath in tissue preparation for transmission electron microscopy. The method used standard reagents and media, and employed ultrasonic bath agitation to accelerate fluid exchange. The liver kidney, stomach and cardiac muscle tissues of male Sprague-Dawley rats were used for the experiment, and the experimental design was divided into 4 groups; The control group using rotators (Traditional method, 1,625 mins) and the three experimental groups using ultrasonic bath (UB) in the primary fixation through the infiltration processes (UB I; 62.5 mins, UB II; 125 mins, UB III; 250 mins). The results were as follows; 1. In the control group, tissues were easily sectioned, and showed well preserved intact membranes, and cell organelles such as mitochondria, lysosome, peroxisome, rough endoplasmic reticulum and smooth endoplasmic reticulum. 2. In the UB treated group I, tissues showed holes due to the inadequate removal of both water and fluids used in the dehydration process. Also the mitochondria of cell organelles, especially, showed swollen intracristal spaces and dense matrices due to poor fixation. 3. In the UB treated group II, tissues showed good preservation of cell organelles and specimen slice sections. Also, no holes were observed. 4. In the UB treated group III, tissues showed leaching of structural components in the cytoplasm, but no holes were observed. In conclusion, the ultrasonic bath procedure takes approximately 120 minutes from specimen fixation to resin infiltration and gives excellent results.

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The Effect of Ultrasonic Vibration in Desizing and Scouring of Polyester Fabrics (폴리에스테르 섬유의 호발과 정련에서 초음파진동 효과)

  • 박영태;최호상;이광수
    • Textile Coloration and Finishing
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    • v.11 no.5
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    • pp.1-6
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    • 1999
  • This study was carried out to investigate the effect of a scouring machine including an ultrasonic system on desizing and scouring polyester fabrics. The ultrasonic frequency of the improved machine showed up at 28.882 kHz. Frequency amplitude increased with the current and the bath temperature, and then showed a constant level. Scouring effect of the ultrasonic machine was better than that of the conventional scouring machine using the mechanical stirring. The ultrasonic machine showed the optimum scouring effect at $50^\circ{C}$ of bath temperature and 10 min. of operation time, as compared to the conventional machine that required operating conditions of high temperature at $90^\circ{C}$, stirring speed at 40 rpm, and stirring time for 15 min..

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Study on the elimination of agricultural chemicals using shower type ultrasonic cleaner (샤워형 초음파 장치를 이용한 농약 제거 효율에 관한 연구)

  • Cho, Sheung-In;Hur, Woong;Kim, Jung-Kuk
    • Proceedings of the KSME Conference
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    • 2003.11a
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    • pp.905-909
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    • 2003
  • This paper describes a shower type ultrasonic cleaning system using particle acceleration, developed for better effectiveness in washing out agricultural chemicals from fruits or vegetables, compared to the existing bath type ultrasonic cleaning system. The shower type system consists of a signal generator, a transducer, and a spouting nozzle, mainly. The system has been tested based on the method recommended by Korea Food and Drug Administration. It is found that shower type system shows better performance and cost-effectiveness than the bath type system that is commercially available .

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Assemblage and Driving Characteristics of a Ultrasonic Fabric Washing Machine (초음파 직물수세기의 구성 및 구동 특성)

  • 이춘길;이광수
    • Textile Coloration and Finishing
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    • v.12 no.3
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    • pp.207-217
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    • 2000
  • A new, high-efficiency ultrasonic fabric washing machine was developed to be an energy-efficient washing machine and to enhance fabric washing quality in washing processes of the dyeing and finishing process in the textile industry. This system is composed of ultrasonic wave generator, air blowing nozzle, torque motor for fabric tension control, and enclosed washing bath, multi-tube type exchanger, noiseless heater, air cylinder, expander roller, mangle upper and lower rollers, bend bar, dancer, shower spray nozzle, and solenoid valve, and so on. These elements are synergised for fabric washing. One of the very important principles is the low tension fabric running system. For an efficient washing effect, a counter flow system is also adopted. The new system also adopts the dancer and torque motor to control fabric tension and prevent fabric creasing. Shower spray nozzle, counter flow and overflow apparatus, and air-blowing apparatus are adopted to enhance the fabric washing effect. In this study, peach yoryu, exter, and moss crepe fabrics were washed by the general and ultrasonic washing systems under different conditions respectively. The washing efficiency was affected by the fabric running speed and characteristics of fabrics. Size content after washing increased with increasing the fabric running speed. The values in the general washing system were higher than those of the ultrasonic washing system. The changes of conductivity in the ultrasonic and the cooling bath were affected by the running time under the ultrasonic generating. The values of conductivity decreased as the experimental time passed.

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Effect of Ultrasonic Wave on the Nickel-Zine Alloy Deposition whit the Variation of Ammonium Chloride Concertration (Ni-Zn 함금도금에서 염화암몬 농도에 따른 초음파의 영향)

  • 양학희;고광진;김재원
    • Journal of the Korean institute of surface engineering
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    • v.21 no.4
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    • pp.168-175
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    • 1988
  • The nickel0zinc allot depositions have been studjen in ammonium chloridw added chloride baths to fine out the effects of ultrasonic irradiation for the electrodeposition processes. The compositions of deposited alloys, the current efficiencies, corrosion resistance and brightness in various conditions of electrodeposition were investigated, in the range of ultrasonic irradiation of 50,500 and 1,000kc/s respectively. The results obtained are as follows; 1. the ratio of nikel to zinc in the deposit increased according 시 the ammonium chloride concentration in irradiated baths. 2. The current efficiencies became also higer in the irradiated bath. 3. Ammonium ions in solution seem to retard formation of zinc hydroxide. 4. The corrsion resistance and brightness of the deposits are dependent upon nickel content of deposits which ranges 10-18%(wt)nickel in the irradiated baths and 11-15%(wt)in ninirradisted baths. 5. The corrosion resistance and brightnes of the deposited are appreciably better in the irradiated baths than in non-irradiated bath with the mole ratio of 3.4(NH+4/Ni+++Zn++).

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Effect of Solution Compositions on Properties of Ni-Fe Nano Thin Film and Wire Made by Electrodeposition Method (Electrodeposition법으로 제조한 Ni-Fe 나노박막 및 나노선의 특성에 미치는 용액 조성의 영향)

  • Koo, Bon-Keup
    • Journal of the Korean institute of surface engineering
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    • v.43 no.5
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    • pp.243-247
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    • 2010
  • The micro Vickers hardness and internal stress of Ni-Fe metal thin film synthesized by electrodeposition method at $25^{\circ}C$ were studied as a function of bath composition, and surface microstructure and atomic compositions of thin films were investigated by SEM and EDS. And the shape change of $200\;{\AA}$ Ni-Fe nanowires made using anodic aluminum oxide(AAO) templates by electrodeposition method were observed by SEM as a function of ultrasonic treatment time and bath composition. The Fe deposition contents on the substrate non-linearly increased with Fe ion concentration over total metal ion concentration. In case of low Fe contents film, the grain size is smaller and denser than high Fe contents deposited films, and the micro Vickers hardness increased with Fe contents of electrodeposited films. These results affected the shape change of nanowire after ultrasonic treatments.

Estimation of Ultrasonic Energy and Sonochemical Effects in Double-Bath-Type Systems and Heterogeneous Systems (이중 반응기 조건 및 비균일계 조건에서의 초음파 에너지 및 화학적 효과 평가)

  • Lee, Hyeon Jae;Son, Younggyu
    • Journal of Soil and Groundwater Environment
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    • v.22 no.5
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    • pp.40-47
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    • 2017
  • The effects of ultrasound in heterogeneous system were investigated in three kinds of ultrasonic systems including a bath-type system (System #1), a double-bath-type system (System #2), and a double-bath-type system partly filled with glass beads (System #3). The ultrasound energy and its attenuation were quantified using calorimetry and the sound pressure measurement method. The sonochemical effects mainly involved in radical oxidation reactions were quantified using KI dosimetry. It was found that ultrasound energy was significantly attenuated in System #2 and #3 due to the presence of solid materials such as a submerged stainless steel reactor and glass beads. However, in spite of low ultrasound energy status, sonochemical oxidation reactions occurred more violently due to the presence of glass beads in System #3. In addition, calorimetry was more adequate to estimate the total energy status of ultrasound in sonoreactors compared to the sound pressure measurement method.

Decomposition of EVA(Ethylene vinyl acetate) used as an adhesion of photovoltaic(PV) module by ultrasonic irradiation in bath-type cleaner (Bath-type 초음파(超音波) 세척기(洗滌器)를 이용(利用)한 태양전지모듈 접착제(接着劑) EVA(Ethylene Vinyl Acetate) 분해특성(分解特性))

  • Kim, Young-Jin;Lee, Jae-Ryeong
    • Resources Recycling
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    • v.20 no.6
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    • pp.50-55
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    • 2011
  • Using ultrasonic irradiation, the separation and recovery of PV cell, made of silicon wafer, from PV module was carried out through selective decomposition of EVA used as an interlaminated binder. The ultrasonic cleaner of bath-type (Output: 130 W, Frequency: 40 kHz) was used as an ultrasonic apparatus in this research. With the fixed distance of 2 cm, from ultrasonic generator to PV cell, the experiment of EVA decomposition was performed in various organic solvents such as Toluene, Trichloroethylene, O-dichlorobenzene, Benzene. And also their concentrations and temperature was changed to survey the optimum conditions. However EVA can be decomposed perfectly at $55^{\circ}C$ within 160 min in 5 M of all kinds of solvent, PV cell may be recovered with being damaged or broken severely. This damage may be resulted from the swelling of EVA in the process of decomposition. Whereas, at the condition of 5 M at $65^{\circ}C$, PV cell can be recovered with the state of minor damage or crack. This implies that the decomposition rate of EVA increases with an increase of temperature, thereby EVA can be decomposed before the swelling of EVA layer. Conclusively, it is possible for PV cell to be recovered within 40 min, at $65^{\circ}C$ in 5 M, with less damage.

Enhancement of bent transfer in the liquid bath by ultrasound (액상용기에서 초음파에 의한 열전달촉진)

  • Kang Won-Jong;Oh Yool-Kwon
    • Proceedings of the KSME Conference
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    • 2002.08a
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    • pp.655-658
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    • 2002
  • The present paper investigated the effect of ultrasonic vibrations on the melting process of a phase-change material (PCM). Furthermore, the present study considered constant heat-flux boundary conditions unlike many of the previous researches, which had adopted constant wall-temperature conditions. Therefore in the study, modified dimensionless numbers such as Stefan and Rayleigh were adopted to represent heat transfer results. The experimental results revealed that ultrasonic vibrations accompanied the effects like agitation, acoustic streaming, cavitation, and oscillating fluid motion, accelerating the melting process as much as 2.5 times, compared with the result of natural melting (i. e., the case without ultrasonic vibration). Such effects are believed to be a prime mechanism in the overall melting process when ultrasonic vibrations were applied. Subsequently, energy could be saved by applying the ultrasonic vibrations to the natural melting In addition, various time-wise dimensionless numbers provided a conclusive evidence of the important role of the ultrasonic vibrations on the melting phenomena of the PCM.

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