Comparative Studies on Two Types Derivatives of Gibberellins for the Gibberellin Analysis by Gas Chromatography-Selected Ion Monitoring

GC-SIM에 의한 두종의 gibberellin유도체의 분석

  • Park, Keun-Hyung (Department of Food Science and Technology, College of Agriculture, Chonnam National University)
  • 박근형 (전남대학교 농과대학 식품가공학과)
  • Published : 1985.06.30

Abstract

Aiming at the improvement of accuracy and sensitivity of gibberellin analysis by gas chromatography-selected ion monitoring (GC-SIM), the mass spectra of two types of 29 gibberellin derivatives, methyl ester-trimethylsilyl ethers and trimethylsilyl ester-trimethylsilyl ethers, were obtained and their advantages and disadvantages in GC-SIM analysis are discussed.

GC-SIM분석법에 의한 GA의 동정 및 정량분석에 대한 정확성과 정출감도의 향상을 목적으로, 29종의 GA를 Me-TMS와 TMS-TMS유도체를 만들고, GC-MS에 의해 이들 유도체의 mass spectra를 측정하였으며, GC-SIM분석에 있어서 Me-TMS유도체와 TMS-TMS유도체의 장단점에 대해 검토하였다.

Keywords