The Korean Journal of Ceramics

The Korean Ceramic Society (한국세라믹학회)
권호 표지

Preparation of Multicomponent Ceramic Powders by Ultrasonic Spray Pyrolysis

  • Youn, Jeong-Han (School of Materials Science and Engineering, Hong-Ik University) ;
  • Chung, Byung-Joo (School of Materials Science and Engineering, Hong-Ik University) ;
  • Sim, Soo-Man (School of Materials Science and Engineering, Hong-Ik University)
  • Published : 2000.03.01
Download PDF
⟨ Previous Next ⟩

Abstract

The preparation of Y-doped $SrZrO_3$powder by ultrasonic spray pyrolysis was investigated as a representative system, in order to produce fine, single phase multicomponent oxide powders. A precursor solution containing metal nitrates, citric acid and ethylene glycol was atomized glycol was atomized with an ultrasonic spray nozzle. Gel particles formed by organic functional groups were pyrolyzed and subsequently calcined at $800^{\circ}C$ to obtain well-crystallized, single perovskite phase. Most of large particles exhibited macroscopic pores and weak agglomeration between primary particles. However, strong agglomeration was observed in the surfaces of large particles. The effect of the microstructures of these particles on size reduction to submicron particles was described.

Keywords

References

  1. Solid State Ionics v.77 Technological Challenges in the Application H. Iwahara
  2. Solid State Ionics v.79 Perovskite Solid Electrolytes: Structure, Transport Properties and Fuel Cell Applications N. Bonanos;K.S. Knight;B. Ellis
  3. Solid State Ionics v.97 On the Development of Proton Conducting Materials for Technological Applications K.D. Kreuer
  4. Solid State Ionics v.77 Comparison of Calcium Doped Barium Cerate Solid Electrolytes Prepared by Different Routes S.D. Flint;R.C.T. Slade
  5. Solid State Ionics v.100 Preparation of Nd-Doped Barium Cerate Through Different Route F. Chen;O.T.S rensen;G. Meng;D. Peng
  6. Korean J. Ceramics v.4 no.3 Preparation of Proton-Conducting Gd-Doped Barium Cerate by Oxalate Coprecipitation Method Y.-S. Choi;S.-M. Sim
  7. Solids State Ionics v.97 Preparation of the High Temparature Proton Conductor Ba₃Ca1.18Nb1.82O8.73 via a Wet Chemical Route E. Zimmer;K. Scharf;T. Mono;J. Frewdrich;T. Schober
  8. Korean J. Ceramics Preparation and Sintering Characteristics of Y-Doped SrZrO₃Powder by Citrate Gel Method Y.-S. Jeon;S.-M. Sim
  9. Mater. Letters v.6 no.427 A Novel Combustion Process for the Synthesis of Fine Particle α-Alumina ad Related Oxide Materials J.J. Kingsley;K.C. Patil
  10. Mater. Letters v.9;10 no.437 Combustion Synthesis of YBa₂-Cu₃-O7-x: Glycine/Metal Nitrates Methods L.R. Pederson;G.D. Maupin;W.J. Weber;D.J. McReady;R.W. Stephens
  11. Ceramic Processing Science Ⅲ Spray Pyrolysis of Multicomponent Ceramic Powders C.B. Martin;R.P. Kurosky;G.D. Maupin;C. Han;J. Javadpour;I.A. Aksay;G.L. Messing(ed.);S. Hirano(ed.);H. Hausner(ed.)
  12. Impact Crystals, X-ray Diffraction B.E. Warren
  13. Am Ceram. Soc. Bull. v.68 no.5 Mixed-Cation Oxide Powders via Polymeric Precursors P.A. Lessing
  14. J. Mater. Sci. v.17 Production of Strontium-Substituted Lanthanum Manganite Preovskite Powder by the Amorphous Citrate Process M.S.G. Baythoun;F.R. Sale
  15. Ceramic Powder Science Ⅱ v.1 Powder Synthesis of SrTiO₃ Boudardy Layer Capacitor Materials B.A. Tuttle;J.A. Voigt;G.L. Messing(ed.);E.R. Fuller, Jr(ed.);H. Hausner(ed.)
  16. J. Mater. Sci. v.27 Barium Titanate Formation by Organic Resins Formed with Mixed Citrate J.P. Coutures;P. Odier;C. Proust
  17. J. Am. Ceram. Soc. v.76 no.11 Ceramic Powder Synthesis by Spray Pyrolysis G.L. Messing;S.-C. Zhang;G.V. Jayanthi