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Scanning Nonlinear Dielectric Microscopy : Overview -A High Resolution Tool for Observing Ferroelectric Domains and Nano-domain Engineering-

  • Cho, Yasuo (Research Institute of Electrical Communication, Tohoku University)
  • Published : 2003.11.01

Abstract

A sub-nanometer resolution Scanning Nonlinear Dielectric Microscope (SNDM) was developed for observing ferroelectric polarization. We also demonstrate that the resolution of SNDM is higher than that of a conventional piezo-response imaging. Secondly, we report new SNDM technique detecting higher nonlinear dielectric constants $\varepsilon$$\_$3333/ and $\varepsilon$$\_$33333/. Higher order nonlinear dielectric imaging provides higher lateral and depth resolution. Finally, the formation of artificial small inverted domain is reported to demonstrate that SNDM system is very useful as a nano-domain engineering tool. The nano-size domain dots were successfully formed in LiTaO$_3$ single crystal. This means that we can obtain a very high density ferroelectric data storage with the density above 1T-bits/inch$^2$.

Keywords

References

  1. Denshi Joho Tsushin Gakkai Ronbunshi v.J78-C-1 no.11 New Microscope for Measuring the Distribution of Nonlinear Dielectric Properties (in Japanese) Y.Cho;A.Kirihara;T.Saeki
  2. Electronics and Communication in Japan v.79 no.6 New Microscope for Measuring the Distribution of Nonlinear Dielectric Properties Y.Cho;A.Kirihara;T.Saeki
  3. Rev. Sci. Instrum v.67 no.6 Scanning Nonlinear Dielectric Microscope Y.Cho;A.Kirihara;T.Saeki https://doi.org/10.1063/1.1146936
  4. Jpn. J. Appl. Phys. v.36 no.5B Scanning Nonlinear Dielectric Microscope Using a Lumped Constant Resonator Probe and Its Application to Investigation of Ferroeletric Polarization Distributions Y.Cho;S.Kirihara;T.Saeki https://doi.org/10.1143/JJAP.36.3152
  5. Appl. Phys. Lett. v.72 no.18 Scanning Nonlinear Dielectric Microscopy with Nanometer Resolution Y.Cho;S.Kazuta;K.Matsuura
  6. Surf. Sci. v.463 Simultaneous Obervation of Nano-sized Ferroelectric Domains and Surface Morphology Using Scanning Nonlinear Dielectric Microscopy H.Odagawa;Y.Cho https://doi.org/10.1016/S0039-6028(00)00636-1
  7. Jpn. J. Appl. Phys. v.39 no.9B Theroetical and Experimental Study on Nanoscale Ferroelecrtic Domain Measurement Using Scanning Nonlinear Dieletric Microscopy H.Odagawa;Y.Cho https://doi.org/10.1143/JJAP.39.5719
  8. Nanotechnology v.8 Scanning Force Microscopy of Domain Structure in Ferroelectric Thin Films : Imaging and Control A.Gruverman;O.Auciello;R.Ramesh;H.Tokumoto https://doi.org/10.1088/0957-4484/8/3A/008
  9. Appl. Phys. Lett. v.74 no.2 Nanoscale Reconstruction of Surface Crystallography from Three-dimensional Polarization Distribution in Ferroelectric Barium-titanate Ceramics L.M.Eng;H.J.Guntherodt;G.A.Schneider;U.Kopke;J.Munoz Saldana https://doi.org/10.1063/1.123266
  10. Jpn. J. of Appl. Phys. v.40 no.5B New Functions of Scanning Nonlinear Dielectric Microscopy Higher-Order Measurement and Vertical Resolution Y.Cho;K.Ohara;A.Koike;H.Odagawa https://doi.org/10.1143/JJAP.40.3544
  11. Jpn. J. Appl. Phys. v.40 no.9B Fundamental Study of Surface Layer on Ferroelectrics by Scanning Nonlinear Dielectric Microscopy K.Ohara;Y.Cho https://doi.org/10.1143/JJAP.40.5833
  12. Appl. Phys. Lett. v.79 no.23 Higher Order Nonlinear Dielectric Microscopy Y.Cho;K.Ohara https://doi.org/10.1063/1.1421645
  13. Appl. Phys. Lett. v.77 no.2 Role of 90° Domains in Lead Zirconate Titanate Thin Films C.S.Ganpule;V.Nagarajan;H.Li;A.S.Ogale;D.E.Steinhauer;S.Aggarwal;E.Willans;R.Ramesh;P.De Wolf https://doi.org/10.1063/1.126954
  14. J. Eur. Ceram. Soc. v.21 Theory of Scanning Nonlinear Dielectric Microscopy and Application to Quantitative Evaluation Y.Cho;K.Ohara;S.Kazuta;H.Odagawa https://doi.org/10.1016/S0955-2219(01)00188-1
  15. Jpn. J. Appl. Phys. v.39 no.9B Theoretical and Experimental Study on Nanoscale Ferroelectric Domain Measurement Using Scanning Nonlinear Dielectric Microscopy H.Odagawa;Y.Cho https://doi.org/10.1143/JJAP.39.5719
  16. J. Phys. Soc. Jpn. v.62 no.3 The 90˚-wall in the Tetragonal Phase of BaTiO₃-type Ferroelectrics Y.Ishibashi https://doi.org/10.1143/JPSJ.62.1044
  17. Jpn. J. of Appl. Phys. v.40 no.5B Measurement of the Ferroelectric Domain Distributions Using Nonliner Dielectric Response and Piezoelectric Response K.Matsuura;Y.Cho;H.Odagawa https://doi.org/10.1143/JJAP.40.3534
  18. J. Cryst. Growth v.197 Stoichiometric LiTaO₃Single Crystal Growth by Double Crucible Czochralski Method Using Automatic Powder Supply System Y.Furukawa;K.Kitamura;E.Suzuki;K.Niwa https://doi.org/10.1016/S0022-0248(98)00921-X
  19. Appl. Phys. Lett. v.73 no.21 Crystal Growth and Low Coercive Field 180˚ Domain Switching Charateristics of Stoichiomertric LiTaO₃ K.Kitamura;Y.Furukawa;K.Niwa;V.Gopalan;T.E.Mitchell https://doi.org/10.1063/1.122676
  20. Solid State Commun. v.109 Switching Kinetics of 180˚ Domains in Congruent LiNbO₃and LiTaO₃Crystals V.Gopalan;T.E.Mitchell;K.E.Sicakfus https://doi.org/10.1016/S0038-1098(98)00509-2
  21. J. Appl. Phys. v.90 no.6 Domain Reversal and Nonstoichiometry in Lithium Tantalate S.Kim;W.Gopalan;K.Kitamura;Y.Furukawa https://doi.org/10.1063/1.1389525