DOI QR코드

DOI QR Code

Green and Hard Machining Characteristics of Zirconia-alumina Composites for Dental Implant

치과 임플란트용 지르코니아-알루미나 복합체의 생 가공 및 경 가공 특성

  • Lim, Hyung-Bong (School of Materials Science and Engineering, Inha University) ;
  • Tang, Dongxu (School of Materials Science and Engineering, Inha University) ;
  • Lee, Ki-Ju (School of Materials Science and Engineering, Inha University) ;
  • Cho, Won-Seung (School of Materials Science and Engineering, Inha University)
  • 임형봉 (인하대학교 신소재공학부) ;
  • 당동욱 (인하대학교 신소재공학부) ;
  • 이기주 (인하대학교 신소재공학부) ;
  • 조원승 (인하대학교 신소재공학부)
  • Received : 2010.12.21
  • Accepted : 2011.02.09
  • Published : 2011.03.31

Abstract

The green and hard machining characteristics of dental ceramics are of great interest to dental industry. The green bodies of TZP/$Al_2O_3$ composites were prepared by the cold isostatic pressing, and machined on the CNC lathe using PCD (polycrystalline diamond) insert under various machining conditions. With increasing nose radius of PCD insert, surface roughness initially increased due to increased cutting resistance, but decreased by the onset of sliding fracture. The lowest surface roughness was obtained at spindle speed of 1,300 rpm and lowest feed rate. Hard bodies were prepared by pressureless sintering the machined green bodies at several temperatures. The grinding test for sintered hard body was conducted using electroplated diamond bur with different grit sizes. During grinding, grain pull out in the composite was occurred due to thermal expansion mismatch between the alumina and zirconia. The strength of the composite decreased with alumina contents, due to increased surface roughness and high monoclinic phase transformed during grinding process. The final polished samples represented high strength by the elimination of a phase transformation layer.

Keywords

References

  1. D. Y. Lee, D. J. Kim, and Y. S. Song, “Chromaticity, Hydrothermal Stability, and Mechanical Properties of $t-ZrO_2/Al_2O_3$ Composites Doped with Yttrium, Niobium, and Ferric Oxides,” Mater. Sci. Eng. A, 289 1-7 (2000). https://doi.org/10.1016/S0921-5093(00)00937-0
  2. R. C. Garvie and P. S. Nicholson, “Phase Analysis in Zirconia Systems,” J. Am. Ceram. Soc., 67 303-5 (1972).
  3. A. V. Virkar and R. L. K. Matsumoto, “Ferroelastic Domain Switching as a Toughening Mechanism in Tetragonal Zirconia,” J. Am. Ceram. Soc., 69 C244-C226 (1986).
  4. S. Lawson, “Review-Environmental Degradation of Zirconia Ceramics,” J. Eur. Ceram. Soc., 15 485-502 (1995). https://doi.org/10.1016/0955-2219(95)00035-S
  5. D. J. Kim, H. J. Jung, and H. J. Kim, “Phase Transformation of Tetragonal Zirconia Alloys by Grinding,” J. Mat. Sci. Lett., 14 285-88 (1995). https://doi.org/10.1007/BF00275625
  6. M. Hirano and H Inada, “Fabrication and Properties of (Y,Ce)-TZP/$Al_2O_3$Composites from Fine Powders Prepared by a Hydrolysis Technique,” J. Ceram. Soc. Jpn., 99 124-30 (1991). https://doi.org/10.2109/jcersj.99.124
  7. D. Y. Lee, D. Kim, and B. Kim, “Influence of Alumina Particle Size on Fracture Toughness of (Y,Nb)-TZP/$Al_2O_3$ Composites,” J. Eur. Ceram. Soc., 22 2173-79 (2002). https://doi.org/10.1016/S0955-2219(02)00012-2
  8. D. J. Kim, M. H. Lee, D. Y. Lee, and J. S. Han, “Mechanical Properties, Phase Stability, and Biocompatibility of (Y,Nb)-TZP/$Al_2O_3$) Composite Abutments for Dental Implant,” J. Biomed. Mater., 53 438-43 (2000). https://doi.org/10.1002/1097-4636(2000)53:4<438::AID-JBM19>3.0.CO;2-3
  9. H. C. Kao and F. Y. Ho, “Surface Machining of Fine-grain Y-TZP,” J. Eur. Ceram. Soc., 20 2447-55 (2000). https://doi.org/10.1016/S0955-2219(00)00114-X
  10. J. H. Song and J. R. G. Evans, “Zirconia/Alumina Functionally Graded Material Made by Ceramic Ink Jet Printing,” J. Eur. Ceram. Soc., 17 1665-73 (1997). https://doi.org/10.1016/S0955-2219(97)00041-1
  11. T. Sato, T. Besshi, and Y. Tada, “Effects of Surface-finishing Condition and Annealing on Transformation Sensitivity of a 3 mol.% $Y_2O_3$ Stabilized Tetragonal Zirconia Surface under Interaction of Lubricant,” Wear, 194 204-11 (1996). https://doi.org/10.1016/0043-1648(95)06867-8
  12. Y. Y. Kim, T. S. Kwak, and K. N. Kim, “Mirror-surface Machining Properties of Structural Ceramics using Diamond Abrasives,” J. Kor. Ceram. Soc., 47 [4] 290-95 (2010) https://doi.org/10.4191/KCERS.2010.47.4.290
  13. J. H. Park, W. J. Lee, and I. S, Kim, “Al2TiO5-machinable Ceramics Made by Reactive Sintering of $Al_2O_3$ and $TiO_2$,” J. Kor. Ceram. Soc., 47 [6] 498-502 (2010) https://doi.org/10.4191/KCERS.2010.47.6.498
  14. H. B. Lim, K. S. Oh, Y. K. Kim, and D. Y. Lee, “Influence of Abrasive Machining and Annealing on Hydrothermal Stability of Zirconia/Alumina Composites as a Hip Joint Head,” Key Eng. Mater., 330-332 1223-26 (2007). https://doi.org/10.4028/www.scientific.net/KEM.330-332.1223
  15. H. B. Lim, K. S. Oh, Y. K. Kim, and D. Y. Lee, “Characteristics of Hydrothermal Stability and Machinability of $t-ZrO_2/Al_2O_3$ Composites as a Femoral Head for Total Hip Replacements,” Mater. Sci. Eng. A, 15 297-301 (2008).
  16. C. Zener, Private Communication to C. S. Smith, “Grains, Phase and Interfaces : An Interpretation of Microstructure,” Am. Inst. Min. Metall. Engrs., 175 15-51 (1949).
  17. N. Louat, “The Resistance to Normal Grain Growth from a Dispersion of Spherical Particles,” Acta Metall., 30 1291-94 (1982). https://doi.org/10.1016/0001-6160(82)90147-X
  18. D. Y. Lee, D. J. Kim, D. Cho, and M. H. Lee, “Effect of $Nb_2O_5\;and\;Y_2O_3$ Alloying on the Mechanical Properties of TZP Ceramics,” Ceram. Intl., 24 461-65 (1998). https://doi.org/10.1016/S0272-8842(97)00036-9