DOI QR코드

DOI QR Code

Surface characteristics of Molybdenum Oxide Films Prepared by Oxidation Thermal Treatment Method

산화 열처리법에 의해 제작된 산화 몰리브데늄 박막의 표면특성 고찰

  • Received : 2014.01.15
  • Accepted : 2014.02.03
  • Published : 2014.03.31

Abstract

In this work, molybdenum oxide films were fabricated by heat-treatment method. Fundamental surface characteristics of molybdenum oxide films were investigated using XRD and Raman spectroscopy. From the results, the optimum MoOx films could be obtained under the conditions of thermal treatment temperature of $550^{\circ}C$, oxidation time of 30 minutes and oxygen flow rate of 250sccm. The thermal treatment method offers a simple and effective route for the synthesis of uniform $MoO_3$ films.

Keywords

References

  1. W. Schmidt, J. Meppelnk, B. Richter, L. E. Kehl, K. Feser, D. Qui, "Behaviour of MO-surge-arrester blocks to fast transients," IEEE Trans. Power Deliv. Vol.4, pp.292-295, 1989. https://doi.org/10.1109/61.19216
  2. I. Kim, et al., "Study of ZnO arrester model for steep front wave," IEEE Trans. Power Deliv. Vol.11, pp.834-837, 1996. https://doi.org/10.1109/61.489341
  3. S. Shichimiya, M. Yamaguchi, N. Furuse, M. Kobayashi, S. Ishibe, "Development of advanced arresters for GIS with new zinc-oxide elements," IEEE Trans. Power Deliv. Vol.13, pp.465-469, 1998. https://doi.org/10.1109/61.660916
  4. Y. M. Sung, "Magnetic null discharge sputtering with full target erosion," Surface and Coatings Technology, Vol.193, pp.123-128, 2005. https://doi.org/10.1016/j.surfcoat.2004.07.122
  5. D. J. Kwak, E. Kuantama, D. W. Han, Y. M. Sung, "Preparation of molybdenum oxide film by a magnetic null discharge sputtering method," Surface and Coatings Technology, Vol.202, pp.5452-5456, 2008. https://doi.org/10.1016/j.surfcoat.2008.06.145
  6. Matteo Ferroni, Vincenzo Guidi, Giuliano Martinelli, Paolo Nel l i , Michele Sacerdot i , Giorgio Sbervegl ier i , "Characterization of a molybdenum oxide sputtered thin film as a gas sensor," Thin Solid Films Vol. 307, pp.148-151. 1997. https://doi.org/10.1016/S0040-6090(97)00279-4
  7. A. Bouzidi, N. Benramdane, H. Tabet-Derraz, C. Mathieu, B. Khelifa, R. Desfeux, "Effect of substrate temperature on the structural and optical properties of $MoO_{3}$ thin films prepared by spray pyrolysis technique," Materials Science and Engineering B Vol.97, pp.5-8, 2003. https://doi.org/10.1016/S0921-5107(02)00385-9
  8. Esmat Abdel-fattah I. Saad, "Dielectric properties of molybdenum oxide thin films," Journal of optoelectronics and Advanced Materials Vol. 7, No. 5, pp.2743-2752, 2005.
  9. R. S. Patil, M. D. Uplane, P. S. Patil, "Electrosynthesis of Electrochromic Molybdenum Oxide Thin Films with Rod-Like Features," Int. J. Electrochem. Sci., Vol.3, pp.259-265, 2008.
  10. Chirakkal V. Krishnan, Rafael Munoz-Espi, Qi Li, Christian Burger and Benjamin Chu, "Formation of molybdenum oxide nanostructures controlled by poly(ethylene oxide)," Chinese Journal of Polymer Science Vol. 27, No. 1, pp.11-22, 2009. https://doi.org/10.1142/S0256767909003613
  11. Y. J. Lee, C. W. Park, D. G. Kim, W. T. Nichols, S. T. Oh, and Y. D. Kim, "$MoO_{3}$ thin film synthesis by chemical vapor transport of volatile $MoO_{3}(OH)_{2}$," Journal of Ceramic Processing Research. Vol. 11, No. 1, pp. 52-55, 2010.